{
  "url": "https://openlegislation.uk/eu-directive-1979-796/annex-II/division-10/division-6/division-6.1",
  "json_url": "https://openlegislation.uk/eu-directive-1979-796/annex-II/division-10/division-6/division-6.1.json",
  "legislation": "eudr/1979/796",
  "legislation_title": "First Commission Directive of 26 July 1979 laying down Community methods of analysis for testing certain sugars intended for human consumption (79/796/EEC)",
  "legislation_url": "https://openlegislation.uk/eu-directive-1979-796",
  "path": "annex/II/division/10/division/6/division/6.1",
  "kind": "division",
  "number": "6.1",
  "heading": "Preparation of the solution",
  "text": "Weigh as quickly as possible 26 ± 0·002 g of the sample and transfer it quantitatively into a 100 ml volumetric flask (5.5) with approximately 60 ml of water.\nDissolve by swirling but without heating.\nWhere clarification is necessary, add 0·5 ml of lead acetate reagent (4.1).\nMix the solution by rotating the flask and wash the flask walls, until the volume is such that the meniscus is about 10 mm below the calibration mark.\nPlace the flask in the water-bath controlled (5.6) at 20 ± 0·1 oC until the temperature of the sugar solution is constant.\nEliminate any bubbles formed at the surface of the liquid with a drop of diethyl ether (4.2).\nMake up to volume with water.\nStopper and mix thoroughly by inverting the flask at least three times.\nAllow to stand for five minutes.",
  "extent": "E+W+S+N.I.",
  "status": null,
  "version": "current",
  "annotations": [],
  "outstanding_effects": [],
  "provenance": {
    "source": "legislation.gov.uk",
    "source_url": "https://www.legislation.gov.uk/eudr/1979/796/annex/II/division/10/division/6/division/6.1",
    "retrieved_at": "2026-11-01T15:23:41.440766+00:00"
  },
  "licence": "Open Government Licence v3.0",
  "licence_url": "https://www.nationalarchives.gov.uk/doc/open-government-licence/version/3/",
  "attribution": "Contains public sector information licensed under the Open Government Licence v3.0. Source: legislation.gov.uk, The National Archives."
}