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Division 6.2.2.1

United Kingdom

Original text. Later amendments are not shown.

Weigh 0,500 g of the sample into a 100 ml round-bottom flask (4.1). Add 30 ml of benzene (4.2) and 20 ml of hydrochloric acid (4.7). Boil the contents of the flask under reflux, with stirring, for 30 minutes.