Division 3 ANNEX V SHALL BE AMENDED AS FOLLOWS:

United Kingdom

1))

The heading shall be replaced by the following:

“TECHNICAL CHARACTERISTICS OF REFERENCE FUEL PRESCRIBED FOR APPROVAL TESTS AND TO VERIFY CONFORMITY OF PRODUCTION

NON-ROAD MOBILE MACHINERY REFERENCE FUEL FOR CI ENGINES TYPE APPROVED TO MEET STAGE I and II LIMIT VALUES AND FOR ENGINES TO BE USED IN INLAND WATERWAY VESSELS.”

2))

The following text shall be inserted after the current table on reference fuel for diesel as follows:

“

NON-ROAD MOBILE MACHINERY REFERENCE FUEL FOR CI ENGINES TYPE APPROVED TO MEET STAGE IIIA LIMIT VALUES.

The values quoted in the specifications are "true values". In establishment of their limit values the terms of ISO 4259 "Petroleum products - Determination and application of precision data in relation to methods of test" have been applied and in fixing a minimum value, a minimum difference of 2R above zero has been taken into account; in fixing a maximum and minimum value, the minimum difference is 4R (R = reproducibility).

Notwithstanding this measure, which is necessary for technical reasons, the manufacturer of fuels should nevertheless aim at a zero value where the stipulated maximum value is 2R and at the mean value in the case of quotations of maximum and minimum limits. Should it be necessary to clarify the questions as to whether a fuel meets the requirements of the specifications, the terms of ISO 4259 should be applied.

The range for cetane number is not in accordance with the requirements of a minimum range of 4R. However, in the case of a dispute between fuel supplier and fuel user, the terms of ISO 4259 may be used to resolve such disputes provided replicate measurements, of sufficient number to archive the necessary precision, are made in preference to single determinatio

The actual sulphur content of the fuel used for the test shall be reported..

Even though oxidation stability is controlled, it is likely that shelf life will be limited. Advice should be sought from the supplier as to storage conditions and life.

Parameter Unit Limits^f1 Test Method
Minimum Maximum
Cetane number^f2 52 54,0 EN-ISO 5165
Density at 15^oC kg/m³ 833 837 EN-ISO 3675
Distillation:
50% point ^oC 245 - EN-ISO 3405
95% point ^oC 345 350 EN-ISO 3405
- Final boiling point ^oC - 370 EN-ISO 3405
Flash point ^oC 55 - EN 22719
CFPP ^oC - -5 EN 116
Viscosity at 40^oC mm²/s 2,5 3,5 EN-ISO 3104
Polycyclic aromatic hydrocarbons % m/m 3,0 6,0 IP 391
Sulphur content^f3 mg/kg - 300 ASTM D 5453
Copper corrosion - class 1 EN-ISO 2160
Conradson carbon residue (10% DR) %m/m - 0,2 EN-ISO 10370
Ash content %m/m - 0,01 EN-ISO 6245
Water content %m/m - 0,05 EN-ISO 12937
Neutralisation (strong acid) number mg KOH/g - 0,02 ASTM D 974
Oxidation stability^f4 mg/ml - 0,025 EN-ISO 12205

NON-ROAD MOBILE MACHINERY REFERENCE FUEL FOR CI ENGINES TYPE APPROVED TO MEET STAGE IIIB AND IV LIMIT VALUES.

Parameter Unit Limits^f5 Test Method
Minimum Maximum
Cetane number^f6 54,0 EN-ISO 5165
Density at 15^oC kg/m³ 833 837 EN-ISO 3675
Distillation:
50% point ^oC 245 - EN-ISO 3405
95% point ^oC 345 350 EN-ISO 3405
- Final boiling point ^oC - 370 EN-ISO 3405
Flash point ^oC 55 - EN 22719
CFPP ^oC - -5 EN 116
Viscosity at 40^oC mm²/s 2,3 3,3 EN-ISO 3104
Polycyclic aromatic hydrocarbons % m/m 3,0 6,0 IP 391
Sulphur content^f7 mg/kg - 10 ASTM D 5453
Copper corrosion - class 1 EN-ISO 2160
Conradson carbon residue (10% DR) % m/m - 0,2 EN-ISO 10370
Ash content % m/m - 0,01 EN-ISO 6245

The values quoted in the specifications are "true values". In establishment of their limit values the terms of ISO 4259 "Petroleum products - Determination and application of precision data in relation to methods of test" have been applied and in fixing a minimum value, a minimum difference of 2R above zero has been taken into account; in fixing a maximum and minimum value, the minimum difference is 4R (R = reproducibility).

Notwithstanding this measure, which is necessary for technical reasons, the manufacturer of fuels should nevertheless aim at a zero value where the stipulated maximum value is 2R and at the mean value in the case of quotations of maximum and minimum limits. Should it be necessary to clarify the questions as to whether a fuel meets the requirements of the specifications, the terms of ISO 4259 should be applied.

The range for cetane number is not in accordance with the requirements of a minimum range of 4R. However, in the case of a dispute between fuel supplier and fuel user, the terms of ISO 4259 may be used to resolve such disputes provided replicate measurements, of sufficient number to archive the necessary precision, are made in preference to single determinations.

The actual sulphur content of the fuel used for the Type I test shall be reported.

Even though oxidation stability is controlled, it is likely that shelf life will be limited. Advice should be sought from the supplier as to storage conditions and life.

Parameter Unit Limits Test Method
Minimum maximum
Water content % m/m - 0,02 EN-ISO 12937
Neutralisation (strong acid) number mg KOH/g - 0,02 ASTM D 974
Oxidation stability^f8 mg/ml - 0,025 EN-ISO 12205
Lubricity (HFRR wear scar diameter at 60^oC) µm - 400 CEC F-06-A-96
FAME prohibited

”

The values quoted in the specifications are "true values". In establishment of their limit values the terms of ISO 4259 "Petroleum products - Determination and application of precision data in relation to methods of test" have been applied and in fixing a minimum value, a minimum difference of 2R above zero has been taken into account; in fixing a maximum and minimum value, the minimum difference is 4R (R = reproducibility). Notwithstanding this measure, which is necessary for technical reasons, the manufacturer of fuels should nevertheless aim at a zero value where the stipulated maximum value is 2R and at the mean value in the case of quotations of maximum and minimum limits. Should it be necessary to clarify the questions as to whether a fuel meets the requirements of the specifications, the terms of ISO 4259 should be applied.
The range for cetane number is not in accordance with the requirements of a minimum range of 4R. However, in the case of a dispute between fuel supplier and fuel user, the terms of ISO 4259 may be used to resolve such disputes provided replicate measurements, of sufficient number to archive the necessary precision, are made in preference to single determinatio
The actual sulphur content of the fuel used for the test shall be reported..
Even though oxidation stability is controlled, it is likely that shelf life will be limited. Advice should be sought from the supplier as to storage conditions and life.
Parameter	Unit	Limits^f1	Test Method
		Minimum	Maximum
Cetane number^f2		52	54,0	EN-ISO 5165
Density at 15^oC	kg/m³	833	837	EN-ISO 3675
Distillation:
50% point	^oC	245	-	EN-ISO 3405
95% point	^oC	345	350	EN-ISO 3405
- Final boiling point	^oC	-	370	EN-ISO 3405
Flash point	^oC	55	-	EN 22719
CFPP	^oC	-	-5	EN 116
Viscosity at 40^oC	mm²/s	2,5	3,5	EN-ISO 3104
Polycyclic aromatic hydrocarbons	% m/m	3,0	6,0	IP 391
Sulphur content^f3	mg/kg	-	300	ASTM D 5453
Copper corrosion		-	class 1	EN-ISO 2160
Conradson carbon residue (10% DR)	%m/m	-	0,2	EN-ISO 10370
Ash content	%m/m	-	0,01	EN-ISO 6245
Water content	%m/m	-	0,05	EN-ISO 12937
Neutralisation (strong acid) number	mg KOH/g	-	0,02	ASTM D 974
Oxidation stability^f4	mg/ml	-	0,025	EN-ISO 12205

NON-ROAD MOBILE MACHINERY REFERENCE FUEL FOR CI ENGINES TYPE APPROVED TO MEET STAGE IIIB AND IV LIMIT VALUES.
Parameter	Unit	Limits^f5	Test Method
Minimum	Maximum
Cetane number^f6			54,0	EN-ISO 5165
Density at 15^oC	kg/m³	833	837	EN-ISO 3675
Distillation:
50% point	^oC	245	-	EN-ISO 3405
95% point	^oC	345	350	EN-ISO 3405
- Final boiling point	^oC	-	370	EN-ISO 3405
Flash point	^oC	55	-	EN 22719
CFPP	^oC	-	-5	EN 116
Viscosity at 40^oC	mm²/s	2,3	3,3	EN-ISO 3104
Polycyclic aromatic hydrocarbons	% m/m	3,0	6,0	IP 391
Sulphur content^f7	mg/kg	-	10	ASTM D 5453
Copper corrosion		-	class 1	EN-ISO 2160
Conradson carbon residue (10% DR)	% m/m	-	0,2	EN-ISO 10370
Ash content	% m/m	-	0,01	EN-ISO 6245

The values quoted in the specifications are "true values". In establishment of their limit values the terms of ISO 4259 "Petroleum products - Determination and application of precision data in relation to methods of test" have been applied and in fixing a minimum value, a minimum difference of 2R above zero has been taken into account; in fixing a maximum and minimum value, the minimum difference is 4R (R = reproducibility). Notwithstanding this measure, which is necessary for technical reasons, the manufacturer of fuels should nevertheless aim at a zero value where the stipulated maximum value is 2R and at the mean value in the case of quotations of maximum and minimum limits. Should it be necessary to clarify the questions as to whether a fuel meets the requirements of the specifications, the terms of ISO 4259 should be applied.
The range for cetane number is not in accordance with the requirements of a minimum range of 4R. However, in the case of a dispute between fuel supplier and fuel user, the terms of ISO 4259 may be used to resolve such disputes provided replicate measurements, of sufficient number to archive the necessary precision, are made in preference to single determinations.
The actual sulphur content of the fuel used for the Type I test shall be reported.
Even though oxidation stability is controlled, it is likely that shelf life will be limited. Advice should be sought from the supplier as to storage conditions and life.
Parameter	Unit	Limits	Test Method
Minimum	maximum
Water content	% m/m	-	0,02	EN-ISO 12937
Neutralisation (strong acid) number	mg KOH/g	-	0,02	ASTM D 974
Oxidation stability^f8	mg/ml	-	0,025	EN-ISO 12205
Lubricity (HFRR wear scar diameter at 60^oC)	µm	-	400	CEC F-06-A-96
FAME	prohibited

Annotations

Footnotes

f1

The values quoted in the specifications are "true values". In establishment of their limit values the terms of ISO 4259 "Petroleum products - Determination and application of precision data in relation to methods of test" have been applied and in fixing a minimum value, a minimum difference of 2R above zero has been taken into account; in fixing a maximum and minimum value, the minimum difference is 4R (R = reproducibility).

Notwithstanding this measure, which is necessary for technical reasons, the manufacturer of fuels should nevertheless aim at a zero value where the stipulated maximum value is 2R and at the mean value in the case of quotations of maximum and minimum limits. Should it be necessary to clarify the questions as to whether a fuel meets the requirements of the specifications, the terms of ISO 4259 should be applied.

f2

The range for cetane number is not in accordance with the requirements of a minimum range of 4R. However, in the case of a dispute between fuel supplier and fuel user, the terms of ISO 4259 may be used to resolve such disputes provided replicate measurements, of sufficient number to archive the necessary precision, are made in preference to single determinatio

f3

The actual sulphur content of the fuel used for the test shall be reported..

f4

Even though oxidation stability is controlled, it is likely that shelf life will be limited. Advice should be sought from the supplier as to storage conditions and life.

f5

f6

f7

The actual sulphur content of the fuel used for the Type I test shall be reported.

f8

Even though oxidation stability is controlled, it is likely that shelf life will be limited. Advice should be sought from the supplier as to storage conditions and life.