{
  "url": "https://openlegislation.uk/eu-regulation-2004-648/annex-VIII/division-5/division-5.4/division-5.4.2",
  "json_url": "https://openlegislation.uk/eu-regulation-2004-648/annex-VIII/division-5/division-5.4/division-5.4.2.json",
  "legislation": "eur/2004/648",
  "legislation_title": "Regulation (EC) No 648/2004 of the European Parliament and of the Council of 31 March 2004 on detergents (Text with EEA relevance)",
  "legislation_url": "https://openlegislation.uk/eu-regulation-2004-648",
  "path": "annex/VIII/division/5/division/5.4/division/5.4.2",
  "kind": "division",
  "number": "5.4.2",
  "heading": null,
  "text": "Add 250 g of the synthetic detergent to be analysed to 1 250 ml ethanol and heat the mixture to boiling point and reflux for one hour with stirring. Pass the hot alcoholic solution through a coarse-pored suction filter heated to 50 ° C and filter rapidly. Wash the flask and suction filter with approximately 200 ml hot ethanol. Collect the filtrate and filter washings in a filter flask.\nIn the case of pastes or liquid products to be analysed, make sure that not more than 25 g anionic surfactants and 35 g soap are contained in the sample. Evaporate this weighed sample to dryness. Dissolve the residue in 500 ml ethanol and proceed as described above.\nIn the case of powders of low apparent density (< 300 g/l) it is recommended to increase the ethanol ratio in the relation 20:1.\nEvaporate the ethanolic filtrate to complete dryness, preferably by means of rotary evaporator. Repeat the operation if a greater quantity of extract is required. Dissolve the residue in 5 000 ml isopropanol/water mixture.",
  "extent": "E+W+S+N.I.",
  "status": null,
  "version": "current",
  "annotations": [],
  "outstanding_effects": [],
  "provenance": {
    "source": "legislation.gov.uk",
    "source_url": "https://www.legislation.gov.uk/eur/2004/648/annex/VIII/division/5/division/5.4/division/5.4.2",
    "retrieved_at": "2026-11-01T14:55:38.850310+00:00"
  },
  "licence": "Open Government Licence v3.0",
  "licence_url": "https://www.nationalarchives.gov.uk/doc/open-government-licence/version/3/",
  "attribution": "Contains public sector information licensed under the Open Government Licence v3.0. Source: legislation.gov.uk, The National Archives."
}