{
  "url": "https://openlegislation.uk/eu-regulation-2009-152",
  "json_url": "https://openlegislation.uk/eu-regulation-2009-152.json",
  "id": "eur/2009/152",
  "title": "Commission Regulation (EC) No 152/2009 of 27 January 2009 laying down the methods of sampling and analysis for the official control of feed (Text with EEA relevance)",
  "short_title": "Regulation (EC) No 152/2009 laying down the methods of sampling and analysis for the official control of feed",
  "long_title": "Commission Regulation (EC) No 152/2009 of 27 January 2009 laying down the methods of sampling and analysis for the official control of feed (Text with EEA relevance)",
  "citation": "EU Regulation No 152/2009",
  "type": "eur",
  "year": "2009",
  "number": "152",
  "version": "current",
  "date": "2009-01-27",
  "revised": false,
  "valid_from": null,
  "extent": "E+W+S+N.I.",
  "unapplied_effects": 8,
  "provisions": [
    {
      "path": "introduction",
      "kind": "introduction",
      "number": null,
      "heading": "Introductory text",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/introduction",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": null
    },
    {
      "path": "article/1",
      "kind": "article",
      "number": "1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/article-1",
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      "parent": null
    },
    {
      "path": "article/2",
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      "url": "https://openlegislation.uk/eu-regulation-2009-152/article-2",
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      "status": null,
      "parent": null
    },
    {
      "path": "article/3",
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      "number": "3",
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      "url": "https://openlegislation.uk/eu-regulation-2009-152/article-3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": null
    },
    {
      "path": "article/4",
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      "url": "https://openlegislation.uk/eu-regulation-2009-152/article-4",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": null
    },
    {
      "path": "article/5",
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      "url": "https://openlegislation.uk/eu-regulation-2009-152/article-5",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": null
    },
    {
      "path": "article/6",
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      "url": "https://openlegislation.uk/eu-regulation-2009-152/article-6",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": null
    },
    {
      "path": "article/7",
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      "url": "https://openlegislation.uk/eu-regulation-2009-152/article-7",
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      "status": null,
      "parent": null
    },
    {
      "path": "signature",
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      "heading": "Signature",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/signature",
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      "status": null,
      "parent": null
    },
    {
      "path": "annex/I",
      "kind": "annex",
      "number": "I",
      "heading": "METHODS OF SAMPLING",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": null
    },
    {
      "path": "annex/I/division/1",
      "kind": "division",
      "number": "1",
      "heading": "PURPOSE AND SCOPE",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I"
    },
    {
      "path": "annex/I/division/2",
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      "number": "2",
      "heading": "DEFINITIONS",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-2",
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      "parent": "annex/I"
    },
    {
      "path": "annex/I/division/3",
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      "number": "3",
      "heading": "GENERAL PROVISIONS",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-3",
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      "status": null,
      "parent": "annex/I"
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    {
      "path": "annex/I/division/4",
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      "heading": "APPARATUS",
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      "status": null,
      "parent": "annex/I"
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    {
      "path": "annex/I/division/4/division/4.1",
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      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-4/division-4.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/4"
    },
    {
      "path": "annex/I/division/4/division/4.2",
      "kind": "division",
      "number": "4.2",
      "heading": "Apparatus recommended for the sampling of solid feed",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/4"
    },
    {
      "path": "annex/I/division/4/division/4.2/division/4.2.1",
      "kind": "division",
      "number": "4.2.1",
      "heading": "Manual sampling",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/4/division/4.2"
    },
    {
      "path": "annex/I/division/4/division/4.2/division/4.2.1/division/4.2.1.1",
      "kind": "division",
      "number": "4.2.1.1",
      "heading": "Flat-bottomed shovel with vertical sides",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/4/division/4.2/division/4.2.1"
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    {
      "path": "annex/I/division/4/division/4.2/division/4.2.1/division/4.2.1.2",
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      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-4/division-4.2/division-4.2.1/division-4.2.1.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/4/division/4.2/division/4.2.1"
    },
    {
      "path": "annex/I/division/4/division/4.2/division/4.2.2",
      "kind": "division",
      "number": "4.2.2",
      "heading": "Mechanical sampling",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-4/division-4.2/division-4.2.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/4/division/4.2"
    },
    {
      "path": "annex/I/division/4/division/4.2/division/4.2.3",
      "kind": "division",
      "number": "4.2.3",
      "heading": "Divider",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-4/division-4.2/division-4.2.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/4/division/4.2"
    },
    {
      "path": "annex/I/division/5",
      "kind": "division",
      "number": "5",
      "heading": "QUANTITATIVE REQUIREMENTS AS REGARDS NUMBER OF INCREMENTAL SAMPLES",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-5",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I"
    },
    {
      "path": "annex/I/division/5/division/5.1",
      "kind": "division",
      "number": "5.1",
      "heading": "Quantitative requirements as regards incremental samples in relation to the control of substances or products uniformly distributed throughout the feed",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/5"
    },
    {
      "path": "annex/I/division/5/division/5.1/division/5.1.1",
      "kind": "division",
      "number": "5.1.1",
      "heading": "Loose solid feed",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-5/division-5.1/division-5.1.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/5/division/5.1"
    },
    {
      "path": "annex/I/division/5/division/5.1/division/5.1.2",
      "kind": "division",
      "number": "5.1.2",
      "heading": "Loose liquid feed",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-5/division-5.1/division-5.1.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/5/division/5.1"
    },
    {
      "path": "annex/I/division/5/division/5.1/division/5.1.3",
      "kind": "division",
      "number": "5.1.3",
      "heading": "Packaged feed",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-5/division-5.1/division-5.1.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/5/division/5.1"
    },
    {
      "path": "annex/I/division/5/division/5.1/division/5.1.4",
      "kind": "division",
      "number": "5.1.4",
      "heading": "Feed blocks and mineral licks",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-5/division-5.1/division-5.1.4",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/5/division/5.1"
    },
    {
      "path": "annex/I/division/5/division/5.1/division/5.1.5",
      "kind": "division",
      "number": "5.1.5",
      "heading": "Roughages/forage",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-5/division-5.1/division-5.1.5",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/5/division/5.1"
    },
    {
      "path": "annex/I/division/5/division/5.2",
      "kind": "division",
      "number": "5.2",
      "heading": "Quantitative requirements as regards incremental samples in relation to the control of constituents or substances likely to be distributed non-uniformly in feed",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-5/division-5.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/5"
    },
    {
      "path": "annex/I/division/5/division/5.3",
      "kind": "division",
      "number": "5.3",
      "heading": "Quantitative requirements as regards the incremental samples in the case of very large lots",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-5/division-5.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/5"
    },
    {
      "path": "annex/I/division/6",
      "kind": "division",
      "number": "6",
      "heading": "QUANTITATIVE REQUIREMENTS AS REGARDS AGGREGATE SAMPLE",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-6",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I"
    },
    {
      "path": "annex/I/division/7",
      "kind": "division",
      "number": "7",
      "heading": "QUANTITATIVE REQUIREMENTS AS REGARDS FINAL SAMPLES",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I"
    },
    {
      "path": "annex/I/division/7/division/1",
      "kind": "division",
      "number": null,
      "heading": "Final samples",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-7/division-1",
      "extent": "E+W+S+N.I.",
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      "parent": "annex/I/division/7"
    },
    {
      "path": "annex/I/division/8",
      "kind": "division",
      "number": "8",
      "heading": "METHOD OF SAMPLING FOR VERY LARGE LOTS OR LOTS STORED OR TRANSPORTED IN A WAY WHEREBY SAMPLING THROUGHOUT THE LOT IS NOT FEASIBLE",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I"
    },
    {
      "path": "annex/I/division/8/division/8.1",
      "kind": "division",
      "number": "8.1",
      "heading": "General principles",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-8/division-8.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/8"
    },
    {
      "path": "annex/I/division/8/division/8.2",
      "kind": "division",
      "number": "8.2",
      "heading": "Large lots transported by ship",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/8"
    },
    {
      "path": "annex/I/division/8/division/8.2/division/8.2.1",
      "kind": "division",
      "number": "8.2.1",
      "heading": "Dynamic sampling of large lots transported by ship",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-8/division-8.2/division-8.2.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/8/division/8.2"
    },
    {
      "path": "annex/I/division/8/division/8.2/division/8.2.2",
      "kind": "division",
      "number": "8.2.2",
      "heading": "Sampling of lots transported by ship by static sampling",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-8/division-8.2/division-8.2.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/8/division/8.2"
    },
    {
      "path": "annex/I/division/8/division/8.3",
      "kind": "division",
      "number": "8.3",
      "heading": "Sampling of large lots stored in warehouses",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-8/division-8.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/8"
    },
    {
      "path": "annex/I/division/8/division/8.4",
      "kind": "division",
      "number": "8.4",
      "heading": "Sampling of storage facilities (silos)",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/8"
    },
    {
      "path": "annex/I/division/8/division/8.4/division/8.4.1",
      "kind": "division",
      "number": "8.4.1",
      "heading": "Sampling of silos (easily) accessible from above",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-8/division-8.4/division-8.4.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/8/division/8.4"
    },
    {
      "path": "annex/I/division/8/division/8.4/division/8.4.2",
      "kind": "division",
      "number": "8.4.2",
      "heading": "Sampling of silos not accessible from above (closed silos)",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/8/division/8.4"
    },
    {
      "path": "annex/I/division/8/division/8.4/division/8.4.2/division/8.4.2.1",
      "kind": "division",
      "number": "8.4.2.1",
      "heading": "Silos not accessible from above (closed silos) with size > 100 tonnes",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-8/division-8.4/division-8.4.2/division-8.4.2.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/8/division/8.4/division/8.4.2"
    },
    {
      "path": "annex/I/division/8/division/8.4/division/8.4.2/division/8.4.2.2",
      "kind": "division",
      "number": "8.4.2.2",
      "heading": "Silos not accessible from above (closed silos) with size < 100 tonnes",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-8/division-8.4/division-8.4.2/division-8.4.2.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/8/division/8.4/division/8.4.2"
    },
    {
      "path": "annex/I/division/8/division/8.5",
      "kind": "division",
      "number": "8.5",
      "heading": "Sampling of loose feed in large closed containers",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-8/division-8.5",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/8"
    },
    {
      "path": "annex/I/division/9",
      "kind": "division",
      "number": "9",
      "heading": "INSTRUCTIONS FOR TAKING, PREPARING AND PACKAGING THE SAMPLES",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I"
    },
    {
      "path": "annex/I/division/9/division/9.1",
      "kind": "division",
      "number": "9.1",
      "heading": "General",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-9/division-9.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/9"
    },
    {
      "path": "annex/I/division/9/division/9.2",
      "kind": "division",
      "number": "9.2",
      "heading": "Incremental samples",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-9/division-9.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/9"
    },
    {
      "path": "annex/I/division/9/division/9.2/division/9.2.1",
      "kind": "division",
      "number": "9.2.1",
      "heading": "Loose feed",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-9/division-9.2/division-9.2.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/9/division/9.2"
    },
    {
      "path": "annex/I/division/9/division/9.2/division/9.2.2",
      "kind": "division",
      "number": "9.2.2",
      "heading": "Packaged feed",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-9/division-9.2/division-9.2.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/9/division/9.2"
    },
    {
      "path": "annex/I/division/9/division/9.2/division/9.2.3",
      "kind": "division",
      "number": "9.2.3",
      "heading": "Homogeneous or homogenisable liquid or semi-liquid feed",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-9/division-9.2/division-9.2.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/9/division/9.2"
    },
    {
      "path": "annex/I/division/9/division/9.2/division/9.2.4",
      "kind": "division",
      "number": "9.2.4",
      "heading": "Non-homogenisable, liquid or semi-liquid feed",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-9/division-9.2/division-9.2.4",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/9/division/9.2"
    },
    {
      "path": "annex/I/division/9/division/9.2/division/9.2.5",
      "kind": "division",
      "number": "9.2.5",
      "heading": "Feed blocks and mineral licks",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-9/division-9.2/division-9.2.5",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/9/division/9.2"
    },
    {
      "path": "annex/I/division/9/division/9.3",
      "kind": "division",
      "number": "9.3",
      "heading": "Preparation of aggregate samples",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-9/division-9.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/9"
    },
    {
      "path": "annex/I/division/9/division/9.4",
      "kind": "division",
      "number": "9.4",
      "heading": "Preparation of final samples",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-I/division-9/division-9.4",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/I/division/9"
    },
    {
      "path": "annex/I/division/9/division/9.5",
      "kind": "division",
      "number": "9.5",
      "heading": "Packaging of samples",
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      "heading": "PREPARATION OF SAMPLES FOR ANALYSIS",
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      "heading": "Precautions to be taken",
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      "path": "annex/III/division/E/division/II/division/4/division/4.1",
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      "path": "annex/III/division/E/division/II/division/5",
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    },
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      "path": "annex/III/division/E/division/II/division/6",
      "kind": "division",
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      "heading": "Calculation of results",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-E/division-II/division-6",
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      "path": "annex/III/division/E/division/II/division/6/division/1",
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      "heading": "Repeatability",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-E/division-II/division-6/division-1",
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    },
    {
      "path": "annex/III/division/F",
      "kind": "division",
      "number": "F",
      "heading": "DETERMINATION OF AMINO ACIDS (EXCEPT TRYPTOPHANE)",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III"
    },
    {
      "path": "annex/III/division/F/division/1",
      "kind": "division",
      "number": "1",
      "heading": "Purpose and scope",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F"
    },
    {
      "path": "annex/III/division/F/division/2",
      "kind": "division",
      "number": "2",
      "heading": "Principle",
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      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F"
    },
    {
      "path": "annex/III/division/F/division/2/division/2.1",
      "kind": "division",
      "number": "2.1",
      "heading": "Free amino acids",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-2/division-2.1",
      "extent": "E+W+S+N.I.",
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      "parent": "annex/III/division/F/division/2"
    },
    {
      "path": "annex/III/division/F/division/2/division/2.2",
      "kind": "division",
      "number": "2.2",
      "heading": "Total amino acids",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-2/division-2.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/2"
    },
    {
      "path": "annex/III/division/F/division/3",
      "kind": "division",
      "number": "3",
      "heading": "Reagents",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.1",
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      "number": "3.1",
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      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.1",
      "extent": "E+W+S+N.I.",
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      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.2",
      "kind": "division",
      "number": "3.2",
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      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.3",
      "kind": "division",
      "number": "3.3",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.4",
      "kind": "division",
      "number": "3.4",
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      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.4",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.5",
      "kind": "division",
      "number": "3.5",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.5",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.6",
      "kind": "division",
      "number": "3.6",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.6",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.7",
      "kind": "division",
      "number": "3.7",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.7",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.8",
      "kind": "division",
      "number": "3.8",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.8",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.9",
      "kind": "division",
      "number": "3.9",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.9",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.10",
      "kind": "division",
      "number": "3.10",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.10",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.11",
      "kind": "division",
      "number": "3.11",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.11",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.12",
      "kind": "division",
      "number": "3.12",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.12",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.13",
      "kind": "division",
      "number": "3.13",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.13",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.14",
      "kind": "division",
      "number": "3.14",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.14",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.15",
      "kind": "division",
      "number": "3.15",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.15",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.16",
      "kind": "division",
      "number": "3.16",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.16",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.16.1",
      "kind": "division",
      "number": "3.16.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.16.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.16.2",
      "kind": "division",
      "number": "3.16.2",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.16.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.16.3",
      "kind": "division",
      "number": "3.16.3",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.16.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.17",
      "kind": "division",
      "number": "3.17",
      "heading": "Sodium hydroxide solution, c = 7,5 mol/l:",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.17",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.18",
      "kind": "division",
      "number": "3.18",
      "heading": "Sodium hydroxide solution, c = 1 mol/l:",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.18",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.19",
      "kind": "division",
      "number": "3.19",
      "heading": "Formic acid — phenol solution:",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.19",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.20",
      "kind": "division",
      "number": "3.20",
      "heading": "Hydrolysis mixture, c = 6 mol HCl/l containing 1 g phenol/l:",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.20",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.21",
      "kind": "division",
      "number": "3.21",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.21",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.22",
      "kind": "division",
      "number": "3.22",
      "heading": "5-Sulfosalicylic acid, ß = 6 %:",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.22",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.23",
      "kind": "division",
      "number": "3.23",
      "heading": "Oxidation mixture (Performic acid — phenol):",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.23",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.24",
      "kind": "division",
      "number": "3.24",
      "heading": "Citrate buffer, c = 0,2 mol Na+/l, pH 2,2:",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.24",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.25",
      "kind": "division",
      "number": "3.25",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.25",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.26",
      "kind": "division",
      "number": "3.26",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.26",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.27",
      "kind": "division",
      "number": "3.27",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.27",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.27.1",
      "kind": "division",
      "number": "3.27.1",
      "heading": "Stock standard solution of amino acids (3.16.1).",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.27.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.27.2",
      "kind": "division",
      "number": "3.27.2",
      "heading": "Stock standard solution of cysteic acid and methionine sulphone, c = 1,25 μmol/ml.",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.27.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.27.3",
      "kind": "division",
      "number": "3.27.3",
      "heading": "Stock standard solution of the internal standard e.g. norleucine, c = 20 μmol/ml.",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.27.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.27.4",
      "kind": "division",
      "number": "3.27.4",
      "heading": "Calibration solution of standard amino acids for use with hydrolysates, c = 5 nmol/50 μl of cysteic acid and methionine sulphone and c = 10 nmol/50 μl of the other amino acids. Dissolve 2,2 g sodium chloride (3.10) in 100 ml beaker with 30 ml citrate buffer (3.24). Add 4,0 ml stock standard solution of amino acids (3.27.1), 4,0 ml stock standard solution of cysteic acid and methionine sulphone (3.27.2) and 0,5 ml stock standard solution of internal standard (3.27.3) if used. Adjust pH to 2,2 with sodium hydroxide (3.18).",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.27.4",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/3/division/3.27.5",
      "kind": "division",
      "number": "3.27.5",
      "heading": "Calibration solution of standard amino acids for use with hydrolysates prepared according to paragraph 5.3.3.1 and for use with extracts (5.2). The calibration solution is prepared according to 3.27.4 but omitting sodium chloride.",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-3/division-3.27.5",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/3"
    },
    {
      "path": "annex/III/division/F/division/4",
      "kind": "division",
      "number": "4",
      "heading": "Apparatus",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F"
    },
    {
      "path": "annex/III/division/F/division/4/division/4.1",
      "kind": "division",
      "number": "4.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-4/division-4.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/4"
    },
    {
      "path": "annex/III/division/F/division/4/division/4.2",
      "kind": "division",
      "number": "4.2",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-4/division-4.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/4"
    },
    {
      "path": "annex/III/division/F/division/4/division/4.3",
      "kind": "division",
      "number": "4.3",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-4/division-4.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/4"
    },
    {
      "path": "annex/III/division/F/division/4/division/4.4",
      "kind": "division",
      "number": "4.4",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-4/division-4.4",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/4"
    },
    {
      "path": "annex/III/division/F/division/4/division/4.5",
      "kind": "division",
      "number": "4.5",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-4/division-4.5",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/4"
    },
    {
      "path": "annex/III/division/F/division/4/division/4.6",
      "kind": "division",
      "number": "4.6",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-4/division-4.6",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/4"
    },
    {
      "path": "annex/III/division/F/division/4/division/4.7",
      "kind": "division",
      "number": "4.7",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-4/division-4.7",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/4"
    },
    {
      "path": "annex/III/division/F/division/4/division/4.8",
      "kind": "division",
      "number": "4.8",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-4/division-4.8",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/4"
    },
    {
      "path": "annex/III/division/F/division/4/division/4.9",
      "kind": "division",
      "number": "4.9",
      "heading": "Amino acid analyser or HPLC equipment with ion exchange column, device for ninhydrin, post column derivatisation and photometric detector.",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-4/division-4.9",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/4"
    },
    {
      "path": "annex/III/division/F/division/5",
      "kind": "division",
      "number": "5",
      "heading": "Procedure",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F"
    },
    {
      "path": "annex/III/division/F/division/5/division/5.1",
      "kind": "division",
      "number": "5.1",
      "heading": "Preparation of the sample",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-5/division-5.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/5"
    },
    {
      "path": "annex/III/division/F/division/5/division/5.2",
      "kind": "division",
      "number": "5.2",
      "heading": "Determination of free amino acids in feed and premixtures",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-5/division-5.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/5"
    },
    {
      "path": "annex/III/division/F/division/5/division/5.3",
      "kind": "division",
      "number": "5.3",
      "heading": "Determination of total amino acids",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/5"
    },
    {
      "path": "annex/III/division/F/division/5/division/5.3/division/5.3.1",
      "kind": "division",
      "number": "5.3.1",
      "heading": "Oxidation",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-5/division-5.3/division-5.3.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/5/division/5.3"
    },
    {
      "path": "annex/III/division/F/division/5/division/5.3/division/5.3.2",
      "kind": "division",
      "number": "5.3.2",
      "heading": "Hydrolysis",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/5/division/5.3"
    },
    {
      "path": "annex/III/division/F/division/5/division/5.3/division/5.3.2/division/5.3.2.1",
      "kind": "division",
      "number": "5.3.2.1",
      "heading": "Hydrolysis of oxidised samples",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-5/division-5.3/division-5.3.2/division-5.3.2.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/5/division/5.3/division/5.3.2"
    },
    {
      "path": "annex/III/division/F/division/5/division/5.3/division/5.3.2/division/5.3.2.2",
      "kind": "division",
      "number": "5.3.2.2",
      "heading": "Hydrolysis of unoxidised samples",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-5/division-5.3/division-5.3.2/division-5.3.2.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/5/division/5.3/division/5.3.2"
    },
    {
      "path": "annex/III/division/F/division/5/division/5.3/division/5.3.2/division/5.3.2.3",
      "kind": "division",
      "number": "5.3.2.3",
      "heading": "Open hydrolysis",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-5/division-5.3/division-5.3.2/division-5.3.2.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/5/division/5.3/division/5.3.2"
    },
    {
      "path": "annex/III/division/F/division/5/division/5.3/division/5.3.2/division/5.3.2.4",
      "kind": "division",
      "number": "5.3.2.4",
      "heading": "Closed Hydrolysis",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-5/division-5.3/division-5.3.2/division-5.3.2.4",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/5/division/5.3/division/5.3.2"
    },
    {
      "path": "annex/III/division/F/division/5/division/5.3/division/5.3.3",
      "kind": "division",
      "number": "5.3.3",
      "heading": "Adjustment of pH",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-5/division-5.3/division-5.3.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/5/division/5.3"
    },
    {
      "path": "annex/III/division/F/division/5/division/5.3/division/5.3.3/division/5.3.3.1",
      "kind": "division",
      "number": "5.3.3.1",
      "heading": "For Chromatographic Systems (4.9) requiring a low sodium concentration",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-5/division-5.3/division-5.3.3/division-5.3.3.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/5/division/5.3/division/5.3.3"
    },
    {
      "path": "annex/III/division/F/division/5/division/5.3/division/5.3.3/division/5.3.3.2",
      "kind": "division",
      "number": "5.3.3.2",
      "heading": "For all other Amino Acid Analysers (4.9)",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-5/division-5.3/division-5.3.3/division-5.3.3.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/5/division/5.3/division/5.3.3"
    },
    {
      "path": "annex/III/division/F/division/5/division/5.3/division/5.3.4",
      "kind": "division",
      "number": "5.3.4",
      "heading": "Sample solution for chromatography",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-5/division-5.3/division-5.3.4",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/5/division/5.3"
    },
    {
      "path": "annex/III/division/F/division/5/division/5.4",
      "kind": "division",
      "number": "5.4",
      "heading": "Chromatography",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-5/division-5.4",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/5"
    },
    {
      "path": "annex/III/division/F/division/6",
      "kind": "division",
      "number": "6",
      "heading": "Calculation of results",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-6",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F"
    },
    {
      "path": "annex/III/division/F/division/6/division/6.1",
      "kind": "division",
      "number": "6.1",
      "heading": "The total dilution volume of extracts (F) for determination of free amino acids (5.2) is calculated as follows:",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-6/division-6.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/6"
    },
    {
      "path": "annex/III/division/F/division/7",
      "kind": "division",
      "number": "7",
      "heading": "Evaluation of the method",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-7",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F"
    },
    {
      "path": "annex/III/division/F/division/7/division/7.1",
      "kind": "division",
      "number": "7.1",
      "heading": "Repeatability",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-7/division-7.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/7"
    },
    {
      "path": "annex/III/division/F/division/7/division/7.2",
      "kind": "division",
      "number": "7.2",
      "heading": "Reproducibility",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-7/division-7.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/7"
    },
    {
      "path": "annex/III/division/F/division/8",
      "kind": "division",
      "number": "8",
      "heading": "Use of reference materials",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-8",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F"
    },
    {
      "path": "annex/III/division/F/division/9",
      "kind": "division",
      "number": "9",
      "heading": "Observations",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F"
    },
    {
      "path": "annex/III/division/F/division/9/division/9.1",
      "kind": "division",
      "number": "9.1",
      "heading": "Because of differences between amino acid analysers the final concentrations of the calibration solutions of standard amino acids (see 3.27.4 and 3.27.5) and of the hydrolysate (see 5.3.4) shall be taken as a guideline.",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-9/division-9.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/9"
    },
    {
      "path": "annex/III/division/F/division/9/division/9.2",
      "kind": "division",
      "number": "9.2",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-9/division-9.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/9"
    },
    {
      "path": "annex/III/division/F/division/9/division/9.3",
      "kind": "division",
      "number": "9.3",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-F/division-9/division-9.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/F/division/9"
    },
    {
      "path": "annex/III/division/G",
      "kind": "division",
      "number": "G",
      "heading": "DETERMINATION OF TRYPTOPHAN",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III"
    },
    {
      "path": "annex/III/division/G/division/1",
      "kind": "division",
      "number": "1",
      "heading": "Purpose and scope",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G"
    },
    {
      "path": "annex/III/division/G/division/2",
      "kind": "division",
      "number": "2",
      "heading": "Principle",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G"
    },
    {
      "path": "annex/III/division/G/division/3",
      "kind": "division",
      "number": "3",
      "heading": "Reagents",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G"
    },
    {
      "path": "annex/III/division/G/division/3/division/3.1",
      "kind": "division",
      "number": "3.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-3/division-3.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/3"
    },
    {
      "path": "annex/III/division/G/division/3/division/3.2",
      "kind": "division",
      "number": "3.2",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-3/division-3.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/3"
    },
    {
      "path": "annex/III/division/G/division/3/division/3.3",
      "kind": "division",
      "number": "3.3",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-3/division-3.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/3"
    },
    {
      "path": "annex/III/division/G/division/3/division/3.4",
      "kind": "division",
      "number": "3.4",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-3/division-3.4",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/3"
    },
    {
      "path": "annex/III/division/G/division/3/division/3.5",
      "kind": "division",
      "number": "3.5",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-3/division-3.5",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/3"
    },
    {
      "path": "annex/III/division/G/division/3/division/3.6",
      "kind": "division",
      "number": "3.6",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-3/division-3.6",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/3"
    },
    {
      "path": "annex/III/division/G/division/3/division/3.7",
      "kind": "division",
      "number": "3.7",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-3/division-3.7",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/3"
    },
    {
      "path": "annex/III/division/G/division/3/division/3.8",
      "kind": "division",
      "number": "3.8",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-3/division-3.8",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/3"
    },
    {
      "path": "annex/III/division/G/division/3/division/3.9",
      "kind": "division",
      "number": "3.9",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-3/division-3.9",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/3"
    },
    {
      "path": "annex/III/division/G/division/3/division/3.10",
      "kind": "division",
      "number": "3.10",
      "heading": "Sodium hydroxide solution, c = 1 mol/l:",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-3/division-3.10",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/3"
    },
    {
      "path": "annex/III/division/G/division/3/division/3.11",
      "kind": "division",
      "number": "3.11",
      "heading": "Hydrochloric acid, c = 6 mol/l:",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-3/division-3.11",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/3"
    },
    {
      "path": "annex/III/division/G/division/3/division/3.12",
      "kind": "division",
      "number": "3.12",
      "heading": "Hydrochloric acid, c = 1 mol/l:",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-3/division-3.12",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/3"
    },
    {
      "path": "annex/III/division/G/division/3/division/3.13",
      "kind": "division",
      "number": "3.13",
      "heading": "Hydrochloric acid, c = 0,1 mol/l:",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-3/division-3.13",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/3"
    },
    {
      "path": "annex/III/division/G/division/3/division/3.14",
      "kind": "division",
      "number": "3.14",
      "heading": "Ortho-phosphoric acid, c = 0,5 mol/l:",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-3/division-3.14",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/3"
    },
    {
      "path": "annex/III/division/G/division/3/division/3.15",
      "kind": "division",
      "number": "3.15",
      "heading": "Concentrated solution of tryptophan (3.2), c = 2,5 μmol/ml:",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-3/division-3.15",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/3"
    },
    {
      "path": "annex/III/division/G/division/3/division/3.16",
      "kind": "division",
      "number": "3.16",
      "heading": "Concentrated internal standard solution, c = 2,5 μmol/ml:",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-3/division-3.16",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/3"
    },
    {
      "path": "annex/III/division/G/division/3/division/3.17",
      "kind": "division",
      "number": "3.17",
      "heading": "Calibration standard solution of tryptophan and internal standard:",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-3/division-3.17",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/3"
    },
    {
      "path": "annex/III/division/G/division/3/division/3.18",
      "kind": "division",
      "number": "3.18",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-3/division-3.18",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/3"
    },
    {
      "path": "annex/III/division/G/division/3/division/3.19",
      "kind": "division",
      "number": "3.19",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-3/division-3.19",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/3"
    },
    {
      "path": "annex/III/division/G/division/3/division/3.20",
      "kind": "division",
      "number": "3.20",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-3/division-3.20",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/3"
    },
    {
      "path": "annex/III/division/G/division/3/division/3.21",
      "kind": "division",
      "number": "3.21",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-3/division-3.21",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/3"
    },
    {
      "path": "annex/III/division/G/division/3/division/3.22",
      "kind": "division",
      "number": "3.22",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-3/division-3.22",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/3"
    },
    {
      "path": "annex/III/division/G/division/4",
      "kind": "division",
      "number": "4",
      "heading": "Apparatus",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G"
    },
    {
      "path": "annex/III/division/G/division/4/division/4.1",
      "kind": "division",
      "number": "4.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-4/division-4.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/4"
    },
    {
      "path": "annex/III/division/G/division/4/division/4.2",
      "kind": "division",
      "number": "4.2",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-4/division-4.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/4"
    },
    {
      "path": "annex/III/division/G/division/4/division/4.3",
      "kind": "division",
      "number": "4.3",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-4/division-4.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/4"
    },
    {
      "path": "annex/III/division/G/division/4/division/4.4",
      "kind": "division",
      "number": "4.4",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-4/division-4.4",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/4"
    },
    {
      "path": "annex/III/division/G/division/4/division/4.5",
      "kind": "division",
      "number": "4.5",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-4/division-4.5",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/4"
    },
    {
      "path": "annex/III/division/G/division/4/division/4.6",
      "kind": "division",
      "number": "4.6",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-4/division-4.6",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/4"
    },
    {
      "path": "annex/III/division/G/division/4/division/4.7",
      "kind": "division",
      "number": "4.7",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-4/division-4.7",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/4"
    },
    {
      "path": "annex/III/division/G/division/4/division/4.8",
      "kind": "division",
      "number": "4.8",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-4/division-4.8",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/4"
    },
    {
      "path": "annex/III/division/G/division/5",
      "kind": "division",
      "number": "5",
      "heading": "Procedure",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G"
    },
    {
      "path": "annex/III/division/G/division/5/division/5.1",
      "kind": "division",
      "number": "5.1",
      "heading": "Preparation of samples",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-5/division-5.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/5"
    },
    {
      "path": "annex/III/division/G/division/5/division/5.2",
      "kind": "division",
      "number": "5.2",
      "heading": "Determination of free tryptophan (extract)",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-5/division-5.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/5"
    },
    {
      "path": "annex/III/division/G/division/5/division/5.3",
      "kind": "division",
      "number": "5.3",
      "heading": "Determination of total tryptophan (hydrolysate)",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-5/division-5.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/5"
    },
    {
      "path": "annex/III/division/G/division/5/division/5.4",
      "kind": "division",
      "number": "5.4",
      "heading": "HPLC determination",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-5/division-5.4",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/5"
    },
    {
      "path": "annex/III/division/G/division/6",
      "kind": "division",
      "number": "6",
      "heading": "Calculation of results",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-6",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G"
    },
    {
      "path": "annex/III/division/G/division/7",
      "kind": "division",
      "number": "7",
      "heading": "Repeatability",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-7",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G"
    },
    {
      "path": "annex/III/division/G/division/8",
      "kind": "division",
      "number": "8",
      "heading": "Results of a collaborative study",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-8",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G"
    },
    {
      "path": "annex/III/division/G/division/9",
      "kind": "division",
      "number": "9",
      "heading": "Observations",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G"
    },
    {
      "path": "annex/III/division/G/division/9/division/9.1",
      "kind": "division",
      "number": "9.1",
      "heading": "Following special chromatographic conditions may give better separation between tryptophan and α-methyl-tryptophan.",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-9/division-9.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/9"
    },
    {
      "path": "annex/III/division/G/division/9/division/9.2",
      "kind": "division",
      "number": "9.2",
      "heading": "The chromatography will vary according to the type of HPLC and column packing material used. The chosen system must be capable of giving baseline separation between the tryptophan and the internal standard. Moreover it is important that degradation products are well separated from the tryptophan and the internal standard. Hydrolysates without internal standard shall be run in order to check the base line under the internal standard for impurities. It is important that the run time is sufficiently long for the elution of all the degradation products, otherwise late eluting peaks may interfere with subsequent chromatographic runs.",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-9/division-9.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/9"
    },
    {
      "path": "annex/III/division/G/division/9/division/9.3",
      "kind": "division",
      "number": "9.3",
      "heading": "Barium hydroxide",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-G/division-9/division-9.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/G/division/9"
    },
    {
      "path": "annex/III/division/H",
      "kind": "division",
      "number": "H",
      "heading": "DETERMINATION OF CRUDE OILS AND FATS",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III"
    },
    {
      "path": "annex/III/division/H/division/1",
      "kind": "division",
      "number": "1",
      "heading": "Purpose and scope",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-H/division-1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H"
    },
    {
      "path": "annex/III/division/H/division/1/division/1.1",
      "kind": "division",
      "number": "1.1",
      "heading": "Procedure A — Directly extractable crude oils and fats",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-H/division-1/division-1.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H/division/1"
    },
    {
      "path": "annex/III/division/H/division/1/division/1.2",
      "kind": "division",
      "number": "1.2",
      "heading": "Procedure B — Total crude oils and fats",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-H/division-1/division-1.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H/division/1"
    },
    {
      "path": "annex/III/division/H/division/1/division/1.3",
      "kind": "division",
      "number": "1.3",
      "heading": "Interpretation of results",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-H/division-1/division-1.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H/division/1"
    },
    {
      "path": "annex/III/division/H/division/2",
      "kind": "division",
      "number": "2",
      "heading": "Principle",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H"
    },
    {
      "path": "annex/III/division/H/division/2/division/2.1",
      "kind": "division",
      "number": "2.1",
      "heading": "Procedure A",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-H/division-2/division-2.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H/division/2"
    },
    {
      "path": "annex/III/division/H/division/2/division/2.2",
      "kind": "division",
      "number": "2.2",
      "heading": "Procedure B",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-H/division-2/division-2.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H/division/2"
    },
    {
      "path": "annex/III/division/H/division/3",
      "kind": "division",
      "number": "3",
      "heading": "Reagents",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H"
    },
    {
      "path": "annex/III/division/H/division/3/division/3.1",
      "kind": "division",
      "number": "3.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-H/division-3/division-3.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H/division/3"
    },
    {
      "path": "annex/III/division/H/division/3/division/3.2",
      "kind": "division",
      "number": "3.2",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-H/division-3/division-3.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H/division/3"
    },
    {
      "path": "annex/III/division/H/division/3/division/3.3",
      "kind": "division",
      "number": "3.3",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-H/division-3/division-3.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H/division/3"
    },
    {
      "path": "annex/III/division/H/division/3/division/3.4",
      "kind": "division",
      "number": "3.4",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-H/division-3/division-3.4",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H/division/3"
    },
    {
      "path": "annex/III/division/H/division/4",
      "kind": "division",
      "number": "4",
      "heading": "Apparatus",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H"
    },
    {
      "path": "annex/III/division/H/division/4/division/4.1",
      "kind": "division",
      "number": "4.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-H/division-4/division-4.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H/division/4"
    },
    {
      "path": "annex/III/division/H/division/4/division/4.2",
      "kind": "division",
      "number": "4.2",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-H/division-4/division-4.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H/division/4"
    },
    {
      "path": "annex/III/division/H/division/4/division/4.3",
      "kind": "division",
      "number": "4.3",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-H/division-4/division-4.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H/division/4"
    },
    {
      "path": "annex/III/division/H/division/5",
      "kind": "division",
      "number": "5",
      "heading": "Procedure",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H"
    },
    {
      "path": "annex/III/division/H/division/5/division/5.1",
      "kind": "division",
      "number": "5.1",
      "heading": "Procedure A (see point 8.1)",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-H/division-5/division-5.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H/division/5"
    },
    {
      "path": "annex/III/division/H/division/5/division/5.2",
      "kind": "division",
      "number": "5.2",
      "heading": "Procedure B",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-H/division-5/division-5.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H/division/5"
    },
    {
      "path": "annex/III/division/H/division/6",
      "kind": "division",
      "number": "6",
      "heading": "Expression of result",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-H/division-6",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H"
    },
    {
      "path": "annex/III/division/H/division/7",
      "kind": "division",
      "number": "7",
      "heading": "Repeatability",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-H/division-7",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H"
    },
    {
      "path": "annex/III/division/H/division/8",
      "kind": "division",
      "number": "8",
      "heading": "Observations",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H"
    },
    {
      "path": "annex/III/division/H/division/8/division/8.1",
      "kind": "division",
      "number": "8.1",
      "heading": "For products with a high content of oils and fats, which are difficult to crush or unsuitable for drawing a homogeneous reduced test sample, proceed as follows.",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-H/division-8/division-8.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H/division/8"
    },
    {
      "path": "annex/III/division/H/division/8/division/8.2",
      "kind": "division",
      "number": "8.2",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-H/division-8/division-8.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H/division/8"
    },
    {
      "path": "annex/III/division/H/division/8/division/8.3",
      "kind": "division",
      "number": "8.3",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-H/division-8/division-8.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H/division/8"
    },
    {
      "path": "annex/III/division/H/division/8/division/8.4",
      "kind": "division",
      "number": "8.4",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-H/division-8/division-8.4",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H/division/8"
    },
    {
      "path": "annex/III/division/H/division/8/division/8.5",
      "kind": "division",
      "number": "8.5",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-H/division-8/division-8.5",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H/division/8"
    },
    {
      "path": "annex/III/division/H/division/8/division/8.6",
      "kind": "division",
      "number": "8.6",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-H/division-8/division-8.6",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/H/division/8"
    },
    {
      "path": "annex/III/division/I",
      "kind": "division",
      "number": "I",
      "heading": "DETERMINATION OF CRUDE FIBRE",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III"
    },
    {
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      "parent": "annex/III/division/J"
    },
    {
      "path": "annex/III/division/J/division/7/division/7.1",
      "kind": "division",
      "number": "7.1",
      "heading": "In the case of feed which are rich in molasses and other feed which are not particularly homogeneous, weigh out 20 g and place with 500 ml of water in a 1 litre volumetric flask. Mix for one hour in the tumbler. Clarify using Carrez 1 (3.2) and II (3.3) reagents as described under 5.1, this time however using four times the quantities of each reagent. Bring up to volume with 80 % ethanol (v/v).",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-J/division-7/division-7.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/J/division/7"
    },
    {
      "path": "annex/III/division/J/division/7/division/7.2",
      "kind": "division",
      "number": "7.2",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-J/division-7/division-7.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/J/division/7"
    },
    {
      "path": "annex/III/division/J/division/8",
      "kind": "division",
      "number": "8",
      "heading": "Observations",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-J/division-8",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/J"
    },
    {
      "path": "annex/III/division/J/division/8/division/8.1",
      "kind": "division",
      "number": "8.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-J/division-8/division-8.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/J/division/8"
    },
    {
      "path": "annex/III/division/J/division/8/division/8.2",
      "kind": "division",
      "number": "8.2",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-J/division-8/division-8.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/J/division/8"
    },
    {
      "path": "annex/III/division/J/division/8/division/8.3",
      "kind": "division",
      "number": "8.3",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-J/division-8/division-8.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/J/division/8"
    },
    {
      "path": "annex/III/division/J/division/8/division/8.3.1",
      "kind": "division",
      "number": "8.3.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-J/division-8/division-8.3.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/J/division/8"
    },
    {
      "path": "annex/III/division/J/division/8/division/8.3.2",
      "kind": "division",
      "number": "8.3.2",
      "heading": "For an accurate calculation of reducing sugars, excluding lactose, the same sample must be used for the two final determinations. One of the analyses is carried out on part of the solution obtained under 5.1, the other on part of the solution obtained during the determination of lactose by the method laid down for that purpose (after fermenting the other types of sugar and clarifying).",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-J/division-8/division-8.3.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/J/division/8"
    },
    {
      "path": "annex/III/division/J/division/8/division/8.3.2/division/1",
      "kind": "division",
      "number": null,
      "heading": "Example:",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-J/division-8/division-8.3.2/division-1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/J/division/8/division/8.3.2"
    },
    {
      "path": "annex/III/division/K",
      "kind": "division",
      "number": "K",
      "heading": "DETERMINATION OF LACTOSE",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III"
    },
    {
      "path": "annex/III/division/K/division/1",
      "kind": "division",
      "number": "1",
      "heading": "Purpose and scope",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-K/division-1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/K"
    },
    {
      "path": "annex/III/division/K/division/2",
      "kind": "division",
      "number": "2",
      "heading": "Principle",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-K/division-2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/K"
    },
    {
      "path": "annex/III/division/K/division/3",
      "kind": "division",
      "number": "3",
      "heading": "Reagents",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/K"
    },
    {
      "path": "annex/III/division/K/division/3/division/3.1",
      "kind": "division",
      "number": "3.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-K/division-3/division-3.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/K/division/3"
    },
    {
      "path": "annex/III/division/K/division/3/division/3.2",
      "kind": "division",
      "number": "3.2",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-K/division-3/division-3.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/K/division/3"
    },
    {
      "path": "annex/III/division/K/division/3/division/3.3",
      "kind": "division",
      "number": "3.3",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-K/division-3/division-3.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/K/division/3"
    },
    {
      "path": "annex/III/division/K/division/3/division/3.4",
      "kind": "division",
      "number": "3.4",
      "heading": "Luff-Schoorl reagent:",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-K/division-3/division-3.4",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/K/division/3"
    },
    {
      "path": "annex/III/division/K/division/3/division/3.4.1",
      "kind": "division",
      "number": "3.4.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-K/division-3/division-3.4.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/K/division/3"
    },
    {
      "path": "annex/III/division/K/division/3/division/3.4.2",
      "kind": "division",
      "number": "3.4.2",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-K/division-3/division-3.4.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/K/division/3"
    },
    {
      "path": "annex/III/division/K/division/3/division/3.4.3",
      "kind": "division",
      "number": "3.4.3",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-K/division-3/division-3.4.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/K/division/3"
    },
    {
      "path": "annex/III/division/K/division/3/division/3.5",
      "kind": "division",
      "number": "3.5",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-K/division-3/division-3.5",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/K/division/3"
    },
    {
      "path": "annex/III/division/K/division/3/division/3.6",
      "kind": "division",
      "number": "3.6",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-K/division-3/division-3.6",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/K/division/3"
    },
    {
      "path": "annex/III/division/K/division/3/division/3.7",
      "kind": "division",
      "number": "3.7",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-K/division-3/division-3.7",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/K/division/3"
    },
    {
      "path": "annex/III/division/K/division/3/division/3.8",
      "kind": "division",
      "number": "3.8",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-K/division-3/division-3.8",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/K/division/3"
    },
    {
      "path": "annex/III/division/K/division/3/division/3.9",
      "kind": "division",
      "number": "3.9",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-K/division-3/division-3.9",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/K/division/3"
    },
    {
      "path": "annex/III/division/K/division/4",
      "kind": "division",
      "number": "4",
      "heading": "Apparatus",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-K/division-4",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/K"
    },
    {
      "path": "annex/III/division/K/division/5",
      "kind": "division",
      "number": "5",
      "heading": "Procedure",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-K/division-5",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/K"
    },
    {
      "path": "annex/III/division/K/division/6",
      "kind": "division",
      "number": "6",
      "heading": "Calculation of results",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-K/division-6",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/K"
    },
    {
      "path": "annex/III/division/K/division/7",
      "kind": "division",
      "number": "7",
      "heading": "Observation",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-K/division-7",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/K"
    },
    {
      "path": "annex/III/division/L",
      "kind": "division",
      "number": "L",
      "heading": "DETERMINATION OF STARCH",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III"
    },
    {
      "path": "annex/III/division/L/division/1",
      "kind": "division",
      "number": null,
      "heading": "POLARIMETRIC METHOD",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/L"
    },
    {
      "path": "annex/III/division/L/division/1/division/1",
      "kind": "division",
      "number": "1",
      "heading": "Purpose and scope",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-L/division-1/division-1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/L/division/1"
    },
    {
      "path": "annex/III/division/L/division/1/division/2",
      "kind": "division",
      "number": "2",
      "heading": "Principle",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-L/division-1/division-2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/L/division/1"
    },
    {
      "path": "annex/III/division/L/division/1/division/3",
      "kind": "division",
      "number": "3",
      "heading": "Reagents",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/L/division/1"
    },
    {
      "path": "annex/III/division/L/division/1/division/3/division/3.1",
      "kind": "division",
      "number": "3.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-L/division-1/division-3/division-3.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/L/division/1/division/3"
    },
    {
      "path": "annex/III/division/L/division/1/division/3/division/3.2",
      "kind": "division",
      "number": "3.2",
      "heading": "Hydrochloric acid. solution 1,13 % (w/v)",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-L/division-1/division-3/division-3.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/L/division/1/division/3"
    },
    {
      "path": "annex/III/division/L/division/1/division/3/division/3.3",
      "kind": "division",
      "number": "3.3",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-L/division-1/division-3/division-3.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/L/division/1/division/3"
    },
    {
      "path": "annex/III/division/L/division/1/division/3/division/3.4",
      "kind": "division",
      "number": "3.4",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-L/division-1/division-3/division-3.4",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/L/division/1/division/3"
    },
    {
      "path": "annex/III/division/L/division/1/division/3/division/3.5",
      "kind": "division",
      "number": "3.5",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-L/division-1/division-3/division-3.5",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/L/division/1/division/3"
    },
    {
      "path": "annex/III/division/L/division/1/division/4",
      "kind": "division",
      "number": "4",
      "heading": "Apparatus",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/L/division/1"
    },
    {
      "path": "annex/III/division/L/division/1/division/4/division/4.1",
      "kind": "division",
      "number": "4.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-L/division-1/division-4/division-4.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/L/division/1/division/4"
    },
    {
      "path": "annex/III/division/L/division/1/division/4/division/4.2",
      "kind": "division",
      "number": "4.2",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-L/division-1/division-4/division-4.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/L/division/1/division/4"
    },
    {
      "path": "annex/III/division/L/division/1/division/5",
      "kind": "division",
      "number": "5",
      "heading": "Procedure",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/L/division/1"
    },
    {
      "path": "annex/III/division/L/division/1/division/5/division/5.1",
      "kind": "division",
      "number": "5.1",
      "heading": "Preparation of the sample",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-L/division-1/division-5/division-5.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/L/division/1/division/5"
    },
    {
      "path": "annex/III/division/L/division/1/division/5/division/5.2",
      "kind": "division",
      "number": "5.2",
      "heading": "Determination of the total optical rotation (P or S) (see observation 7.1)",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-L/division-1/division-5/division-5.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/L/division/1/division/5"
    },
    {
      "path": "annex/III/division/L/division/1/division/5/division/5.3",
      "kind": "division",
      "number": "5.3",
      "heading": "Determination of the optical rotation (P' or S') of substances soluble in 40 % ethanol",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-L/division-1/division-5/division-5.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/L/division/1/division/5"
    },
    {
      "path": "annex/III/division/L/division/1/division/6",
      "kind": "division",
      "number": "6",
      "heading": "Calculation of results",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-L/division-1/division-6",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/L/division/1"
    },
    {
      "path": "annex/III/division/L/division/1/division/6/division/6.1",
      "kind": "division",
      "number": "6.1",
      "heading": "Measurement by polarimeter",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-L/division-1/division-6/division-6.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/L/division/1/division/6"
    },
    {
      "path": "annex/III/division/L/division/1/division/6/division/6.2",
      "kind": "division",
      "number": "6.2",
      "heading": "Measurement by saccharimeter",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-L/division-1/division-6/division-6.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/L/division/1/division/6"
    },
    {
      "path": "annex/III/division/L/division/1/division/6/division/6.3",
      "kind": "division",
      "number": "6.3",
      "heading": "Repeatability",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-L/division-1/division-6/division-6.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/L/division/1/division/6"
    },
    {
      "path": "annex/III/division/L/division/1/division/7",
      "kind": "division",
      "number": "7",
      "heading": "Observations",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/L/division/1"
    },
    {
      "path": "annex/III/division/L/division/1/division/7/division/7.1",
      "kind": "division",
      "number": "7.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-L/division-1/division-7/division-7.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/L/division/1/division/7"
    },
    {
      "path": "annex/III/division/L/division/1/division/7/division/7.2",
      "kind": "division",
      "number": "7.2",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-III/division-L/division-1/division-7/division-7.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/III/division/L/division/1/division/7"
    },
    {
      "path": "annex/III/division/L/division/1/division/7/division/7.3",
      "kind": "division",
      "number": "7.3",
      "heading": "The following feed materials, where they are present in significant amounts in feed, are known to give rise to interferences when determining the starch content by the polarimetric method and thereby incorrect results could be yielded:",
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      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-B/division-5/division-5.6/division-5.6.1/division-5.6.1.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/B/division/5/division/5.6/division/5.6.1"
    },
    {
      "path": "annex/IV/division/B/division/5/division/5.6/division/5.6.1/division/5.6.1.2",
      "kind": "division",
      "number": "5.6.1.2",
      "heading": "Preparation of the calibration solutions and calibration graph",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-B/division-5/division-5.6/division-5.6.1/division-5.6.1.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/B/division/5/division/5.6/division/5.6.1"
    },
    {
      "path": "annex/IV/division/B/division/5/division/5.6/division/5.6.1/division/5.6.1.3",
      "kind": "division",
      "number": "5.6.1.3",
      "heading": "UV standardisation of the DL-α-tocopherol acetate stock solution (3.10.1)",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-B/division-5/division-5.6/division-5.6.1/division-5.6.1.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/B/division/5/division/5.6/division/5.6.1"
    },
    {
      "path": "annex/IV/division/B/division/5/division/5.6/division/5.6.2",
      "kind": "division",
      "number": "5.6.2",
      "heading": "DL-α-tocopherol standard",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/B/division/5/division/5.6"
    },
    {
      "path": "annex/IV/division/B/division/5/division/5.6/division/5.6.2/division/5.6.2.1",
      "kind": "division",
      "number": "5.6.2.1",
      "heading": "Preparation of the working standard solution",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-B/division-5/division-5.6/division-5.6.2/division-5.6.2.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/B/division/5/division/5.6/division/5.6.2"
    },
    {
      "path": "annex/IV/division/B/division/5/division/5.6/division/5.6.2/division/5.6.2.2",
      "kind": "division",
      "number": "5.6.2.2",
      "heading": "Preparation of the calibration solutions and calibration graph",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-B/division-5/division-5.6/division-5.6.2/division-5.6.2.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/B/division/5/division/5.6/division/5.6.2"
    },
    {
      "path": "annex/IV/division/B/division/5/division/5.6/division/5.6.2/division/5.6.2.3",
      "kind": "division",
      "number": "5.6.2.3",
      "heading": "UV standardisation of the DL-α-tocopherol stock solution (3.11.1)",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-B/division-5/division-5.6/division-5.6.2/division-5.6.2.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/B/division/5/division/5.6/division/5.6.2"
    },
    {
      "path": "annex/IV/division/B/division/6",
      "kind": "division",
      "number": "6",
      "heading": "Calculation of the results",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-B/division-6",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/B"
    },
    {
      "path": "annex/IV/division/B/division/7",
      "kind": "division",
      "number": "7",
      "heading": "Observations",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/B"
    },
    {
      "path": "annex/IV/division/B/division/7/division/7.1",
      "kind": "division",
      "number": "7.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-B/division-7/division-7.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/B/division/7"
    },
    {
      "path": "annex/IV/division/B/division/7/division/7.2",
      "kind": "division",
      "number": "7.2",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-B/division-7/division-7.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/B/division/7"
    },
    {
      "path": "annex/IV/division/B/division/7/division/7.3",
      "kind": "division",
      "number": "7.3",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-B/division-7/division-7.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/B/division/7"
    },
    {
      "path": "annex/IV/division/B/division/7/division/7.4",
      "kind": "division",
      "number": "7.4",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-B/division-7/division-7.4",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/B/division/7"
    },
    {
      "path": "annex/IV/division/B/division/7/division/7.5",
      "kind": "division",
      "number": "7.5",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-B/division-7/division-7.5",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/B/division/7"
    },
    {
      "path": "annex/IV/division/B/division/7/division/7.6",
      "kind": "division",
      "number": "7.6",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-B/division-7/division-7.6",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/B/division/7"
    },
    {
      "path": "annex/IV/division/B/division/7/division/7.7",
      "kind": "division",
      "number": "7.7",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-B/division-7/division-7.7",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/B/division/7"
    },
    {
      "path": "annex/IV/division/B/division/7/division/7.8",
      "kind": "division",
      "number": "7.8",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-B/division-7/division-7.8",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/B/division/7"
    },
    {
      "path": "annex/IV/division/B/division/7/division/7.9",
      "kind": "division",
      "number": "7.9",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-B/division-7/division-7.9",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/B/division/7"
    },
    {
      "path": "annex/IV/division/B/division/8",
      "kind": "division",
      "number": "8",
      "heading": "Repeatability·",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-B/division-8",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/B"
    },
    {
      "path": "annex/IV/division/B/division/9",
      "kind": "division",
      "number": "9",
      "heading": "Results of a collaborative study",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-B/division-9",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/B"
    },
    {
      "path": "annex/IV/division/C",
      "kind": "division",
      "number": "C",
      "heading": "DETERMINATION OF THE TRACE ELEMENTS IRON, COPPER, MANGANESE AND ZINC",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV"
    },
    {
      "path": "annex/IV/division/C/division/1",
      "kind": "division",
      "number": "1",
      "heading": "Purpose and scope",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-C/division-1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C"
    },
    {
      "path": "annex/IV/division/C/division/2",
      "kind": "division",
      "number": "2",
      "heading": "Principle",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-C/division-2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C"
    },
    {
      "path": "annex/IV/division/C/division/3",
      "kind": "division",
      "number": "3",
      "heading": "Reagents",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C"
    },
    {
      "path": "annex/IV/division/C/division/3/division/1",
      "kind": "division",
      "number": null,
      "heading": "Introductory comments",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-C/division-3/division-1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/3"
    },
    {
      "path": "annex/IV/division/C/division/3/division/3.1",
      "kind": "division",
      "number": "3.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-C/division-3/division-3.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/3"
    },
    {
      "path": "annex/IV/division/C/division/3/division/3.2",
      "kind": "division",
      "number": "3.2",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-C/division-3/division-3.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/3"
    },
    {
      "path": "annex/IV/division/C/division/3/division/3.3",
      "kind": "division",
      "number": "3.3",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-C/division-3/division-3.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/3"
    },
    {
      "path": "annex/IV/division/C/division/3/division/3.4",
      "kind": "division",
      "number": "3.4",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-C/division-3/division-3.4",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/3"
    },
    {
      "path": "annex/IV/division/C/division/3/division/3.5",
      "kind": "division",
      "number": "3.5",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-C/division-3/division-3.5",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/3"
    },
    {
      "path": "annex/IV/division/C/division/3/division/3.6",
      "kind": "division",
      "number": "3.6",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-C/division-3/division-3.6",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/3"
    },
    {
      "path": "annex/IV/division/C/division/3/division/3.7",
      "kind": "division",
      "number": "3.7",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-C/division-3/division-3.7",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/3"
    },
    {
      "path": "annex/IV/division/C/division/3/division/3.7.1",
      "kind": "division",
      "number": "3.7.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-C/division-3/division-3.7.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/3"
    },
    {
      "path": "annex/IV/division/C/division/3/division/3.8",
      "kind": "division",
      "number": "3.8",
      "heading": "Standard copper solution (1 000 μg Cu/ml) prepared as follows or equivalent commercially available solution:",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-C/division-3/division-3.8",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/3"
    },
    {
      "path": "annex/IV/division/C/division/3/division/3.8.1",
      "kind": "division",
      "number": "3.8.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-C/division-3/division-3.8.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/3"
    },
    {
      "path": "annex/IV/division/C/division/3/division/3.9",
      "kind": "division",
      "number": "3.9",
      "heading": "Standard manganese solution (1 000 μg Mn/ml) prepared as follows or equivalent commercially available solution:",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-C/division-3/division-3.9",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/3"
    },
    {
      "path": "annex/IV/division/C/division/3/division/3.9.1",
      "kind": "division",
      "number": "3.9.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-C/division-3/division-3.9.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/3"
    },
    {
      "path": "annex/IV/division/C/division/3/division/3.10",
      "kind": "division",
      "number": "3.10",
      "heading": "Standard zinc solution (1 000 μg Zn/ml) prepared as follows or equivalent commercially available solution:",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-C/division-3/division-3.10",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/3"
    },
    {
      "path": "annex/IV/division/C/division/3/division/3.10.1",
      "kind": "division",
      "number": "3.10.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-C/division-3/division-3.10.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/3"
    },
    {
      "path": "annex/IV/division/C/division/3/division/3.11",
      "kind": "division",
      "number": "3.11",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-C/division-3/division-3.11",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/3"
    },
    {
      "path": "annex/IV/division/C/division/4",
      "kind": "division",
      "number": "4",
      "heading": "Apparatus",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C"
    },
    {
      "path": "annex/IV/division/C/division/4/division/4.1",
      "kind": "division",
      "number": "4.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-C/division-4/division-4.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/4"
    },
    {
      "path": "annex/IV/division/C/division/4/division/4.2",
      "kind": "division",
      "number": "4.2",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-C/division-4/division-4.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/4"
    },
    {
      "path": "annex/IV/division/C/division/4/division/4.3",
      "kind": "division",
      "number": "4.3",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-C/division-4/division-4.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/4"
    },
    {
      "path": "annex/IV/division/C/division/5",
      "kind": "division",
      "number": "5",
      "heading": "Procedure",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C"
    },
    {
      "path": "annex/IV/division/C/division/5/division/5.1",
      "kind": "division",
      "number": "5.1",
      "heading": "Samples containing organic matter",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/5"
    },
    {
      "path": "annex/IV/division/C/division/5/division/5.1/division/5.1.1",
      "kind": "division",
      "number": "5.1.1",
      "heading": "Ashing and preparation of the solution for analysis",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/5/division/5.1"
    },
    {
      "path": "annex/IV/division/C/division/5/division/5.1/division/5.1.1/division/5.1.1.1",
      "kind": "division",
      "number": "5.1.1.1",
      "heading": "Place 5 to 10 g of sample weighed to the nearest 0,2 mg in a quartz or platinum crucible (see Note (b)), dry in an oven at 105 oC and introduce the crucible into the cold muffle furnace (4.1). Close the furnace (see Note (c)) and gradually raise the temperature to 450 to 475 oC over about 90 minutes. Maintain this temperature for 4 to 16 hours (e.g. overnight) to remove carbonaceous material and then open the furnace and allow to cool (see Note (d)).",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-C/division-5/division-5.1/division-5.1.1/division-5.1.1.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/5/division/5.1/division/5.1.1"
    },
    {
      "path": "annex/IV/division/C/division/5/division/5.1/division/5.1.1/division/5.1.1.2",
      "kind": "division",
      "number": "5.1.1.2",
      "heading": "If the residue in the filter appears black (carbon), put it back in the furnace and ash again at 450 to 475 oC. This ashing, which only requires a few hours (about three to five hours), is complete when the ash appears white or nearly white. Dissolve the residue with about 2 ml of hydrochloric acid (3.1), evaporate to dryness and add 5 ml of 6 mol/litre hydrochloric acid (3.2). Heat, filter the solution into the volumetric flask and make up to the mark with water (HCl concentration about 0,5 mol/litre.",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/5/division/5.1/division/5.1.1"
    },
    {
      "path": "annex/IV/division/C/division/5/division/5.1/division/5.1.1/division/5.1.1.2/annotation/1",
      "kind": "division",
      "number": null,
      "heading": "Notes:",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-C/division-5/division-5.1/division-5.1.1/division-5.1.1.2/annotation/1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/5/division/5.1/division/5.1.1/division/5.1.1.2"
    },
    {
      "path": "annex/IV/division/C/division/5/division/5.1/division/5.1.2",
      "kind": "division",
      "number": "5.1.2",
      "heading": "Spectrophotometric determination",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/C/division/5/division/5.1"
    },
    {
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    {
      "path": "annex/IV/division/D/division/5/division/5.1/division/5.1.1",
      "kind": "division",
      "number": "5.1.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-D/division-5/division-5.1/division-5.1.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/D/division/5/division/5.1"
    },
    {
      "path": "annex/IV/division/D/division/5/division/5.1/division/5.1.2",
      "kind": "division",
      "number": "5.1.2",
      "heading": "A recovery test shall be carried out by analysing the blank feed which has been fortified by addition of a quantity of halofuginone, similar to that present in the sample. To fortify at a level of 3 mg/kg, add 300 μl of the stock standard solution (3.6.1) to 10 g of the blank feed, mix and wait for 10 minutes before proceeding with the extraction step (5.2).",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-D/division-5/division-5.1/division-5.1.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/D/division/5/division/5.1"
    },
    {
      "path": "annex/IV/division/D/division/5/division/5.2",
      "kind": "division",
      "number": "5.2",
      "heading": "Extraction",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-D/division-5/division-5.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/D/division/5"
    },
    {
      "path": "annex/IV/division/D/division/5/division/5.3",
      "kind": "division",
      "number": "5.3",
      "heading": "Clean up",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/D/division/5"
    },
    {
      "path": "annex/IV/division/D/division/5/division/5.3/division/5.3.1",
      "kind": "division",
      "number": "5.3.1",
      "heading": "Preparation of the Amberlite column",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-D/division-5/division-5.3/division-5.3.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/D/division/5/division/5.3"
    },
    {
      "path": "annex/IV/division/D/division/5/division/5.3/division/5.3.2",
      "kind": "division",
      "number": "5.3.2",
      "heading": "Sample clean up",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-D/division-5/division-5.3/division-5.3.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/D/division/5/division/5.3"
    },
    {
      "path": "annex/IV/division/D/division/5/division/5.4",
      "kind": "division",
      "number": "5.4",
      "heading": "HPLC determination",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/D/division/5"
    },
    {
      "path": "annex/IV/division/D/division/5/division/5.4/division/5.4.1",
      "kind": "division",
      "number": "5.4.1",
      "heading": "Parameters",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-D/division-5/division-5.4/division-5.4.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/D/division/5/division/5.4"
    },
    {
      "path": "annex/IV/division/D/division/5/division/5.4/division/5.4.2",
      "kind": "division",
      "number": "5.4.2",
      "heading": "Calibration graph",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-D/division-5/division-5.4/division-5.4.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/D/division/5/division/5.4"
    },
    {
      "path": "annex/IV/division/D/division/5/division/5.4/division/5.4.3",
      "kind": "division",
      "number": "5.4.3",
      "heading": "Sample solution",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-D/division-5/division-5.4/division-5.4.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/D/division/5/division/5.4"
    },
    {
      "path": "annex/IV/division/D/division/6",
      "kind": "division",
      "number": "6",
      "heading": "Calculation of results",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-D/division-6",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/D"
    },
    {
      "path": "annex/IV/division/D/division/7",
      "kind": "division",
      "number": "7",
      "heading": "Validation of the results",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/D"
    },
    {
      "path": "annex/IV/division/D/division/7/division/7.1",
      "kind": "division",
      "number": "7.1",
      "heading": "Identity",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-D/division-7/division-7.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/D/division/7"
    },
    {
      "path": "annex/IV/division/D/division/7/division/7.1/division/7.1.1",
      "kind": "division",
      "number": "7.1.1",
      "heading": "Co-chromatography",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-D/division-7/division-7.1/division-7.1.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/D/division/7/division/7.1"
    },
    {
      "path": "annex/IV/division/D/division/7/division/7.1/division/7.1.2",
      "kind": "division",
      "number": "7.1.2",
      "heading": "Diode-array detection",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-D/division-7/division-7.1/division-7.1.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/D/division/7/division/7.1"
    },
    {
      "path": "annex/IV/division/D/division/7/division/7.2",
      "kind": "division",
      "number": "7.2",
      "heading": "Repeatability",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-D/division-7/division-7.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/D/division/7"
    },
    {
      "path": "annex/IV/division/D/division/7/division/7.3",
      "kind": "division",
      "number": "7.3",
      "heading": "Recovery",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-D/division-7/division-7.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/D/division/7"
    },
    {
      "path": "annex/IV/division/D/division/8",
      "kind": "division",
      "number": "8",
      "heading": "Results of a collaborative study",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-D/division-8",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/D"
    },
    {
      "path": "annex/IV/division/E",
      "kind": "division",
      "number": "E",
      "heading": "DETERMINATION OF ROBENIDINE",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV"
    },
    {
      "path": "annex/IV/division/E/division/1",
      "kind": "division",
      "number": "1",
      "heading": "Purpose and scope",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E"
    },
    {
      "path": "annex/IV/division/E/division/2",
      "kind": "division",
      "number": "2",
      "heading": "Principle",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E"
    },
    {
      "path": "annex/IV/division/E/division/3",
      "kind": "division",
      "number": "3",
      "heading": "Reagents",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E"
    },
    {
      "path": "annex/IV/division/E/division/3/division/3.1",
      "kind": "division",
      "number": "3.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-3/division-3.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/3"
    },
    {
      "path": "annex/IV/division/E/division/3/division/3.2",
      "kind": "division",
      "number": "3.2",
      "heading": "Acidified methanol.",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-3/division-3.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/3"
    },
    {
      "path": "annex/IV/division/E/division/3/division/3.3",
      "kind": "division",
      "number": "3.3",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-3/division-3.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/3"
    },
    {
      "path": "annex/IV/division/E/division/3/division/3.4",
      "kind": "division",
      "number": "3.4",
      "heading": "Molecular sieve.",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-3/division-3.4",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/3"
    },
    {
      "path": "annex/IV/division/E/division/3/division/3.5",
      "kind": "division",
      "number": "3.5",
      "heading": "Aluminium oxide acidic activity grade I for column chromatography.",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-3/division-3.5",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/3"
    },
    {
      "path": "annex/IV/division/E/division/3/division/3.6",
      "kind": "division",
      "number": "3.6",
      "heading": "Potassium dihydrogen phosphate solution, c = 0,025 mol/l.",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-3/division-3.6",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/3"
    },
    {
      "path": "annex/IV/division/E/division/3/division/3.7",
      "kind": "division",
      "number": "3.7",
      "heading": "Di-sodium hydrogen phosphate solution, c = 0,025 mol/l.",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-3/division-3.7",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/3"
    },
    {
      "path": "annex/IV/division/E/division/3/division/3.8",
      "kind": "division",
      "number": "3.8",
      "heading": "HPLC mobile phase.",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-3/division-3.8",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/3"
    },
    {
      "path": "annex/IV/division/E/division/3/division/3.9",
      "kind": "division",
      "number": "3.9",
      "heading": "Standard substance.",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-3/division-3.9",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/3"
    },
    {
      "path": "annex/IV/division/E/division/3/division/3.9.1",
      "kind": "division",
      "number": "3.9.1",
      "heading": "Robenidine stock standard solution: 300 μg/ml",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-3/division-3.9.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/3"
    },
    {
      "path": "annex/IV/division/E/division/3/division/3.9.2",
      "kind": "division",
      "number": "3.9.2",
      "heading": "Robenidine intermediate standard solution: 12 μg/ml",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-3/division-3.9.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/3"
    },
    {
      "path": "annex/IV/division/E/division/3/division/3.9.3",
      "kind": "division",
      "number": "3.9.3",
      "heading": "Calibration solutions",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-3/division-3.9.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/3"
    },
    {
      "path": "annex/IV/division/E/division/3/division/3.10",
      "kind": "division",
      "number": "3.10",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-3/division-3.10",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/3"
    },
    {
      "path": "annex/IV/division/E/division/4",
      "kind": "division",
      "number": "4",
      "heading": "Apparatus",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E"
    },
    {
      "path": "annex/IV/division/E/division/4/division/4.1",
      "kind": "division",
      "number": "4.1",
      "heading": "Glass column.",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-4/division-4.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/4"
    },
    {
      "path": "annex/IV/division/E/division/4/division/4.2",
      "kind": "division",
      "number": "4.2",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-4/division-4.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/4"
    },
    {
      "path": "annex/IV/division/E/division/4/division/4.3",
      "kind": "division",
      "number": "4.3",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-4/division-4.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/4"
    },
    {
      "path": "annex/IV/division/E/division/4/division/4.4",
      "kind": "division",
      "number": "4.4",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-4/division-4.4",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/4"
    },
    {
      "path": "annex/IV/division/E/division/4/division/4.4.1",
      "kind": "division",
      "number": "4.4.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-4/division-4.4.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/4"
    },
    {
      "path": "annex/IV/division/E/division/4/division/4.5",
      "kind": "division",
      "number": "4.5",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-4/division-4.5",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/4"
    },
    {
      "path": "annex/IV/division/E/division/4/division/4.6",
      "kind": "division",
      "number": "4.6",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-4/division-4.6",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/4"
    },
    {
      "path": "annex/IV/division/E/division/4/division/4.7",
      "kind": "division",
      "number": "4.7",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-4/division-4.7",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/4"
    },
    {
      "path": "annex/IV/division/E/division/5",
      "kind": "division",
      "number": "5",
      "heading": "Procedure",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E"
    },
    {
      "path": "annex/IV/division/E/division/5/annotation/1",
      "kind": "division",
      "number": null,
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-5/annotation/1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/5"
    },
    {
      "path": "annex/IV/division/E/division/5/division/5.1",
      "kind": "division",
      "number": "5.1",
      "heading": "General",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/5"
    },
    {
      "path": "annex/IV/division/E/division/5/division/5.1/division/5.1.1",
      "kind": "division",
      "number": "5.1.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-5/division-5.1/division-5.1.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/5/division/5.1"
    },
    {
      "path": "annex/IV/division/E/division/5/division/5.1/division/5.1.2",
      "kind": "division",
      "number": "5.1.2",
      "heading": "A recovery test shall be carried out by analysing the blank feed (5.1.1) which has been fortified by addition of a quantity of robenidine, similar to that present in the sample. To fortify at a level of 60 mg/kg, transfer 3,0 ml of the stock standard solution (3.9.1) to a 250 ml conical flask. Evaporate the solution to ca. 0,5 ml in a stream of nitrogen. Add 15 g of the blank feed, mix and wait for 10 minutes before proceeding with the extraction step (5.2).",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-5/division-5.1/division-5.1.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/5/division/5.1"
    },
    {
      "path": "annex/IV/division/E/division/5/division/5.2",
      "kind": "division",
      "number": "5.2",
      "heading": "Extraction",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-5/division-5.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/5"
    },
    {
      "path": "annex/IV/division/E/division/5/division/5.3",
      "kind": "division",
      "number": "5.3",
      "heading": "Purification",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/5"
    },
    {
      "path": "annex/IV/division/E/division/5/division/5.3/division/5.3.1",
      "kind": "division",
      "number": "5.3.1",
      "heading": "Preparation of the aluminium-oxide column",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-E/division-5/division-5.3/division-5.3.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/IV/division/E/division/5/division/5.3"
    },
    {
      "path": "annex/IV/division/E/division/5/division/5.3/division/5.3.2",
      "kind": "division",
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      "heading": "Sample purification",
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      "number": "7.1.1",
      "heading": "Co-chromatography",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-IV/division-G/division-7/division-7.1/division-7.1.1",
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      "path": "annex/IV/division/G/division/7/division/7.3",
      "kind": "division",
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      "heading": "Recovery",
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      "path": "annex/IV/division/G/division/8",
      "kind": "division",
      "number": "8",
      "heading": "Results of a collaborative study",
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      "extent": "E+W+S+N.I.",
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      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
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    },
    {
      "path": "annex/V/division/A",
      "kind": "division",
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      "heading": "DETERMINATION OF FREE AND TOTAL GOSSYPOL",
      "url": null,
      "extent": "E+W+S+N.I.",
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      "parent": "annex/V/division/A"
    },
    {
      "path": "annex/V/division/A/division/3",
      "kind": "division",
      "number": "3",
      "heading": "Reagents",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/V/division/A"
    },
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      "path": "annex/V/division/A/division/3/division/3.1",
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      "path": "annex/V/division/A/division/3/division/3.4",
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      "path": "annex/V/division/A/division/3/division/3.6",
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      "heading": "Apparatus",
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      "heading": "Test sample",
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      "path": "annex/V/division/A/division/6/division/6.2",
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      "number": "3",
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      "number": "CHAPTER II",
      "heading": "Sample preparation and requirements for methods of analysis used in offical control of the levels of dioxins (PCDD/Fs) and dioxin-like PCBs in feed",
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      "heading": "METHODS OF ANALYSIS TO CONTROL ILLEGAL PRESENCE OF NO LONGER AUTHORISED ADDITIVES IN FEED",
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      "path": "annex/VIII/division/A/division/3/division/3.6",
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      "number": "5.4",
      "heading": "Ion-exchange chromatography",
      "url": null,
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      "path": "annex/VIII/division/A/division/5/division/5.4/division/5.4.1",
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      "number": "5.4.1",
      "heading": "Preparation of the cation-exchange column",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-A/division-5/division-5.4/division-5.4.1",
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      "path": "annex/VIII/division/A/division/5/division/5.4/division/5.4.2",
      "kind": "division",
      "number": "5.4.2",
      "heading": "Column chromatography",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-A/division-5/division-5.4/division-5.4.2",
      "extent": "E+W+S+N.I.",
      "status": null,
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    {
      "path": "annex/VIII/division/A/division/5/division/5.5",
      "kind": "division",
      "number": "5.5",
      "heading": "Liquid-liquid partition",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-A/division-5/division-5.5",
      "extent": "E+W+S+N.I.",
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      "parent": "annex/VIII/division/A/division/5"
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      "path": "annex/VIII/division/A/division/5/division/5.6",
      "kind": "division",
      "number": "5.6",
      "heading": "HPLC determination",
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      "path": "annex/VIII/division/A/division/5/division/5.6/division/5.6.1",
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      "number": "5.6.1",
      "heading": "Parameters",
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      "path": "annex/VIII/division/A/division/5/division/5.6/division/5.6.2",
      "kind": "division",
      "number": "5.6.2",
      "heading": "Calibration graph",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-A/division-5/division-5.6/division-5.6.2",
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      "path": "annex/VIII/division/A/division/5/division/5.6/division/5.6.3",
      "kind": "division",
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      "heading": "Sample solution",
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      "path": "annex/VIII/division/A/division/6",
      "kind": "division",
      "number": "6",
      "heading": "Calculation of results",
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    {
      "path": "annex/VIII/division/A/division/7",
      "kind": "division",
      "number": "7",
      "heading": "Validation of the results",
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      "status": null,
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      "path": "annex/VIII/division/A/division/7/division/7.1",
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      "heading": "Identity",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-A/division-7/division-7.1",
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      "parent": "annex/VIII/division/A/division/7"
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      "path": "annex/VIII/division/A/division/7/division/7.1/division/7.1.1",
      "kind": "division",
      "number": "7.1.1",
      "heading": "Co-chromatography",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-A/division-7/division-7.1/division-7.1.1",
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      "status": null,
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      "path": "annex/VIII/division/A/division/7/division/7.1/division/7.1.2",
      "kind": "division",
      "number": "7.1.2",
      "heading": "Diode-array detection",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-A/division-7/division-7.1/division-7.1.2",
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      "parent": "annex/VIII/division/A/division/7/division/7.1"
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      "path": "annex/VIII/division/A/division/7/division/7.2",
      "kind": "division",
      "number": "7.2",
      "heading": "Repeatability",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-A/division-7/division-7.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/VIII/division/A/division/7"
    },
    {
      "path": "annex/VIII/division/A/division/7/division/7.3",
      "kind": "division",
      "number": "7.3",
      "heading": "Recovery",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-A/division-7/division-7.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/VIII/division/A/division/7"
    },
    {
      "path": "annex/VIII/division/A/division/8",
      "kind": "division",
      "number": "8",
      "heading": "Results of a collaborative study",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-A/division-8",
      "extent": "E+W+S+N.I.",
      "status": null,
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    },
    {
      "path": "annex/VIII/division/B",
      "kind": "division",
      "number": "B",
      "heading": "DETERMINATION OF OLAQUINDOX",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-B",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/VIII"
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      "path": "annex/VIII/division/B/division/1",
      "kind": "division",
      "number": "1",
      "heading": "Purpose and scope",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-B/division-1",
      "extent": "E+W+S+N.I.",
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      "parent": "annex/VIII/division/B"
    },
    {
      "path": "annex/VIII/division/B/division/2",
      "kind": "division",
      "number": "2",
      "heading": "Principle",
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      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/VIII/division/B"
    },
    {
      "path": "annex/VIII/division/B/division/3",
      "kind": "division",
      "number": "3",
      "heading": "Reagents",
      "url": null,
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/VIII/division/B"
    },
    {
      "path": "annex/VIII/division/B/division/3/division/3.1",
      "kind": "division",
      "number": "3.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-B/division-3/division-3.1",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/VIII/division/B/division/3"
    },
    {
      "path": "annex/VIII/division/B/division/3/division/3.2",
      "kind": "division",
      "number": "3.2",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-B/division-3/division-3.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/VIII/division/B/division/3"
    },
    {
      "path": "annex/VIII/division/B/division/3/division/3.3",
      "kind": "division",
      "number": "3.3",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-B/division-3/division-3.3",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/VIII/division/B/division/3"
    },
    {
      "path": "annex/VIII/division/B/division/3/division/3.4",
      "kind": "division",
      "number": "3.4",
      "heading": "Mobile phase for HPLC.",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-B/division-3/division-3.4",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/VIII/division/B/division/3"
    },
    {
      "path": "annex/VIII/division/B/division/3/division/3.5",
      "kind": "division",
      "number": "3.5",
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      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-B/division-3/division-3.5",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/VIII/division/B/division/3"
    },
    {
      "path": "annex/VIII/division/B/division/3/division/3.5.1",
      "kind": "division",
      "number": "3.5.1",
      "heading": "Olaquindox stock standard solution, 250 μg/ml",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-B/division-3/division-3.5.1",
      "extent": "E+W+S+N.I.",
      "status": null,
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    },
    {
      "path": "annex/VIII/division/B/division/3/division/3.5.2",
      "kind": "division",
      "number": "3.5.2",
      "heading": "Olaquindox intermediate standard solution, 25 μg/ml",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-B/division-3/division-3.5.2",
      "extent": "E+W+S+N.I.",
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    {
      "path": "annex/VIII/division/B/division/3/division/3.5.3",
      "kind": "division",
      "number": "3.5.3",
      "heading": "Calibration solutions",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-B/division-3/division-3.5.3",
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      "kind": "division",
      "number": "4",
      "heading": "Apparatus",
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      "parent": "annex/VIII/division/B"
    },
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      "path": "annex/VIII/division/B/division/4/division/4.1",
      "kind": "division",
      "number": "4.1",
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      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-B/division-4/division-4.1",
      "extent": "E+W+S+N.I.",
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    },
    {
      "path": "annex/VIII/division/B/division/4/division/4.2",
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      "number": "4.2",
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      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-B/division-4/division-4.2",
      "extent": "E+W+S+N.I.",
      "status": null,
      "parent": "annex/VIII/division/B/division/4"
    },
    {
      "path": "annex/VIII/division/B/division/4/division/4.3",
      "kind": "division",
      "number": "4.3",
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      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-B/division-4/division-4.3",
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    },
    {
      "path": "annex/VIII/division/B/division/4/division/4.3.1",
      "kind": "division",
      "number": "4.3.1",
      "heading": null,
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-B/division-4/division-4.3.1",
      "extent": "E+W+S+N.I.",
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    },
    {
      "path": "annex/VIII/division/B/division/4/division/4.4",
      "kind": "division",
      "number": "4.4",
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    },
    {
      "path": "annex/VIII/division/B/division/5",
      "kind": "division",
      "number": "5",
      "heading": "Procedure",
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    },
    {
      "path": "annex/VIII/division/B/division/5/annotation/1",
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    },
    {
      "path": "annex/VIII/division/B/division/5/division/5.1",
      "kind": "division",
      "number": "5.1",
      "heading": "General",
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      "path": "annex/VIII/division/B/division/5/division/5.1/division/5.1.1",
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      "number": "5.1.1",
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      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-B/division-5/division-5.1/division-5.1.1",
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      "path": "annex/VIII/division/B/division/5/division/5.1/division/5.1.2",
      "kind": "division",
      "number": "5.1.2",
      "heading": "A recovery test shall be carried out by analysing the blank feed which has been fortified by addition of a quantity of olaquindox, similar to that present in the sample. To fortify at a level of 50 mg/kg, transfer 10,0 ml of the stock standard solution (3.5.1) to a 250 ml conical flask and evaporate the solution to ca. 0,5 ml. Add 50 g of the blank feed, mix thoroughly and leave for 10 min. mixing again several times before proceeding with the extraction step (5.2).",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-B/division-5/division-5.1/division-5.1.2",
      "extent": "E+W+S+N.I.",
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    },
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      "path": "annex/VIII/division/B/division/5/division/5.2",
      "kind": "division",
      "number": "5.2",
      "heading": "Extraction",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-B/division-5/division-5.2",
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    },
    {
      "path": "annex/VIII/division/B/division/5/division/5.3",
      "kind": "division",
      "number": "5.3",
      "heading": "HPLC determination",
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      "path": "annex/VIII/division/B/division/5/division/5.3/division/5.3.1",
      "kind": "division",
      "number": "5.3.1",
      "heading": "Parameters:",
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      "path": "annex/VIII/division/B/division/5/division/5.3/division/5.3.2",
      "kind": "division",
      "number": "5.3.2",
      "heading": "Calibration graph",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-B/division-5/division-5.3/division-5.3.2",
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      "path": "annex/VIII/division/B/division/5/division/5.3/division/5.3.3",
      "kind": "division",
      "number": "5.3.3",
      "heading": "Sample solution",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-B/division-5/division-5.3/division-5.3.3",
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      "number": "6",
      "heading": "Calculation of the results",
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      "heading": "Validation of the results",
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      "status": null,
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    },
    {
      "path": "annex/VIII/division/B/division/7/division/7.1",
      "kind": "division",
      "number": "7.1",
      "heading": "Identity",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-B/division-7/division-7.1",
      "extent": "E+W+S+N.I.",
      "status": null,
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    {
      "path": "annex/VIII/division/B/division/7/division/7.1/division/7.1.1",
      "kind": "division",
      "number": "7.1.1",
      "heading": "Co-chromatography",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-B/division-7/division-7.1/division-7.1.1",
      "extent": "E+W+S+N.I.",
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      "path": "annex/VIII/division/B/division/7/division/7.1/division/7.1.2",
      "kind": "division",
      "number": "7.1.2",
      "heading": "Diode array detection",
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    },
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      "number": "7.2",
      "heading": "Repeatability",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-B/division-7/division-7.2",
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    },
    {
      "path": "annex/VIII/division/B/division/7/division/7.3",
      "kind": "division",
      "number": "7.3",
      "heading": "Recovery",
      "url": "https://openlegislation.uk/eu-regulation-2009-152/annex-VIII/division-B/division-7/division-7.3",
      "extent": "E+W+S+N.I.",
      "status": null,
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      "path": "annex/VIII/division/B/division/8",
      "kind": "division",
      "number": "8",
      "heading": "Results of a collaborative study",
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      "extent": "E+W+S+N.I.",
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    {
      "path": "annex/VIII/division/B/division/9",
      "kind": "division",
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