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Division 5.1.2 A recovery test shall be carried out by analysing the blank feed (5.1.1) which has been fortified by addition of a quantity of robenidine, similar to that present in the sample. To fortify at a level of 60 mg/kg, transfer 3,0 ml of the stock standard solution (3.9.1) to a 250 ml conical flask. Evaporate the solution to ca. 0,5 ml in a stream of nitrogen. Add 15 g of the blank feed, mix and wait for 10 minutes before proceeding with the extraction step (5.2).

United Kingdom

Original text. Later amendments are not shown.

Note:
  • For the purpose of this method, the blank feed shall be similar in type to that of the sample and on analysis robenidine shall not be detected.