Division 8 Results of a collaborative study
United Kingdom
A collaborative studyf1 was arranged in which 2 premixtures (samples 1 and 2) and 5 feeds (samples 3-7) were analysed by 12 laboratories. Duplicate analyses were performed on each sample. The results are given in the following table:
Content declared by manufacturer. | |||||||
Feed prepared in the laboratory. | |||||||
| Sample 1Chicken premix | Sample 2Turkey premix | Sample 3Turkey pellets | Sample 4Chicken crumbs | Sample 5Turkey Feed | Sample 6Poultry Feed A | Sample 7Poultry Feed B | |
|---|---|---|---|---|---|---|---|
| L | 12 | 12 | 12 | 12 | 12 | 12 | 12 |
| n | 23 | 23 | 23 | 23 | 23 | 23 | 23 |
| Mean [mg/kg] | 5 050 | 16 200 | 76,5 | 78,4 | 92,9 | 48,3 | 32,6 |
| sr [mg/kg] | 107 | 408 | 1,71 | 2,23 | 2,27 | 1,93 | 1,75 |
| CVr [%] | 2,12 | 2,52 | 2,24 | 2,84 | 2,44 | 4,0 | 5,37 |
| sR [mg/kg] | 286 | 883 | 3,85 | 7,32 | 5,29 | 3,47 | 3,49 |
| CVR [%] | 5,66 | 5,45 | 5,03 | 9,34 | 5,69 | 7,18 | 10,7 |
| Nominal content [mg/kg] | 5 000f2 | 16 000 | 80 | 105 | 120 | 50f3 | 35 |
L n sr sR CVr CVR
number of laboratories
number of single results
standard deviation of repeatability
standard deviation of reproducibility
coefficient of variation of repeatability, %
coefficient of variation of reproducibility, %.
Annotations
Footnotes
- f1
-
Analyst, 1995, 120, 2175-2180.
- f2
Content declared by manufacturer.
- f3
Feed prepared in the laboratory.