Division 1.4 PRINCIPLE OF THE TEST METHOD
United Kingdom
A number of representative core samples are taken from the fibre blanket or from loose bulk fibre. The bulk fibres are reduced in length using a crushing procedure and a representative sub-sample dispersed in water. Aliquots are extracted and filtered through a 0,2 μm pore size, polycarbonate filter and prepared for examination using scanning electron microscope (SEM) techniques. The fibre diameters are measured at a screen magnification of × 10 000 or greaterf1 using a line intercept method to give an unbiased estimate of the median diameter. The lower 95 % confidence interval (based on a one sided test) is calculated to give an estimate of the lowest value of the geometric mean fibre diameter of the material.
Annotations
Footnotes
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This magnification value is indicated for 3 µm fibres, for 6 µm fibres a magnification of × 5 000 may be more suitable.