Paragraph 8 REMARK
If the presence of lumps is observed after sieving, the analysis should be carried out again in the following way:
Slowly pour 50 g of the sample into a 1 litre flask containing 500 ml of the sodium hexametaphosphate solution, stirring continuously. Stopper the flask and shake vigorously by hand to break up the lumps. Transfer the whole suspension into the top sieve and wash the flask thoroughly. Continue the analysis as described under paragraph 6.