{
  "url": "https://openlegislation.uk/fertilisers-sampling-and-analysis-regulations-northern-ireland-1996/schedule-2/part-I/chapter-25i./paragraph-4",
  "json_url": "https://openlegislation.uk/fertilisers-sampling-and-analysis-regulations-northern-ireland-1996/schedule-2/part-I/chapter-25i./paragraph-4.json",
  "legislation": "nisr/1996/513",
  "legislation_title": "Fertilisers (Sampling and Analysis) Regulations (Northern Ireland) 1996",
  "legislation_url": "https://openlegislation.uk/fertilisers-sampling-and-analysis-regulations-northern-ireland-1996",
  "path": "schedule/2/part/I/chapter/25i./paragraph/4",
  "kind": "paragraph",
  "number": "4",
  "heading": "REAGENTS",
  "text": "Hydrochloric acid solution, about 6 M\n4.1 See Method 25d (4.1).\nHydrochloric acid solution, about 0.5 M\n4.2 See Method 25d (4.2).\nLanthanum salt solutions (10 g of La per litre)\n4.3 See Method 25d (4.3).\nManganese calibration solutions\n4.4 Manganese stock solution (1000 μg/ml)\n4.4.1 In a 250 ml beaker, weigh to the nearest 0.1 mg, 1 g of manganese, add 25 ml of 6 M hydrochloric acid solution (4.1). Heat on a hot plate until the manganese is completely dissolved. When cool, transfer quantitatively to a 1000 ml volumetric flask. Make up to volume with water and mix thoroughly.\nManganese working solution (100 μg/ml)\n4.4.2 Place 20 ml of the stock solution (4.4.1) in a 200 ml volumetric flask. Make up to volume with the 0.5 M hydrochloric acid solution (4.2) and mix thoroughly.",
  "extent": null,
  "status": null,
  "version": "current",
  "annotations": [],
  "outstanding_effects": [],
  "provenance": {
    "source": "legislation.gov.uk",
    "source_url": "https://www.legislation.gov.uk/nisr/1996/513/schedule/2/part/I/chapter/25i./paragraph/4",
    "retrieved_at": "2026-10-29T02:32:40.012993+00:00"
  },
  "licence": "Open Government Licence v3.0",
  "licence_url": "https://www.nationalarchives.gov.uk/doc/open-government-licence/version/3/",
  "attribution": "Contains public sector information licensed under the Open Government Licence v3.0. Source: legislation.gov.uk, The National Archives."
}