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Commission Directive of 25 July 1980 relating to the Community method of analysis for determining the erucic acid content in oils and fats intended to be used as such for human consumption and foodstuffs containing added oils or fats (80/891/EEC) (repealed)

EU Directive 1980/891 · Adopted 25 July 1980 · Extends to United Kingdom

Original text. legislation.gov.uk does not revise this item, so later amendments are not shown here. Changes made to it are listed under each provision when known.

Commission Directive

of 25 July 1980

relating to the Community method of analysis for determining the erucic acid content in oils and fats intended to be used as such for human consumption and foodstuffs containing added oils or fats

(80/891/EEC) (repealed)

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Annotations to the whole text

Textual amendments

F1

Repealed by Commission Regulation (EU) 2015/705 of 30 April 2015 laying down methods of sampling and performance criteria for the methods of analysis for the official control of the levels of erucic acid in foodstuffs and repealing Commission Directive 80/891/EEC (Text with EEA relevance).

Contents

  1. 1Article 1 Repealed
  2. 2Article 2 Repealed
  3. 3Article 3 Repealed
  4. 4Article 4 Repealed
  5. Signature
  6. Annex: THE DETERMINATION OF THE ERUCIC ACID CONTENT IN OILS AND FATS INTENDED TO BE USED AS SUCH FOR HUMAN CONSUMPTION AND IN THE FAT OR OIL COMPONENT OF FOODSTUFFS TO WHICH OILS OR FATS HAVE BEEN ADDED Repealed
  7. INTRODUCTION Repealed
  8. SAMPLE PREPARATION Repealed
  9. 1.1General Repealed
  10. 1.2Preparation of the sample for analysis in the laboratory Repealed
  11. 1.3Containers Repealed
  12. REAGENTS Repealed
  13. Water Repealed
  14. 2.1.1Division 2.1.1 Repealed
  15. 2.1.2Division 2.1.2 Repealed
  16. 2.2Chemicals Repealed
  17. APPARATUS Repealed
  18. 3.1List of apparatus Repealed
  19. 3.2Analytical balance Repealed
  20. EXPRESSION OF THE RESULTS Repealed
  21. 4.1Results Repealed
  22. 4.2Calculation of the percentage Repealed
  23. 4.3Number of significant figures Repealed
  24. DETERMINATION OF ERUCIC ACID Repealed
  25. 1SCOPE AND FIELD OF APPLICATION Repealed
  26. 2DEFINITION Repealed
  27. 3PRINCIPLE Repealed
  28. REAGENTS Repealed
  29. 4.1Division 4.1 Repealed
  30. 4.2Division 4.2 Repealed
  31. 4.3Division 4.3 Repealed
  32. 4.4Division 4.4 Repealed
  33. 4.5Division 4.5 Repealed
  34. 4.6Division 4.6 Repealed
  35. 4.7Division 4.7 Repealed
  36. 4.8Division 4.8 Repealed
  37. 4.9Division 4.9 Repealed
  38. APPARATUS Repealed
  39. 5.1Apparatus for thin-layer chromatography to include, in particular: Repealed
  40. 5.2Division 5.2 Repealed
  41. PROCEDURE Repealed
  42. 6.1Preparation of fatty-acid methyl esters Repealed
  43. Thin-layer chromatography Repealed
  44. 6.2.1Preparation of plates Repealed
  45. 6.2.2Application of methyl esters Repealed
  46. 6.2.3Development of the plates Repealed
  47. 6.2.4Separation of the methyl ester fractions Repealed
  48. Gas-liquid chromatography Repealed
  49. 6.3.1Division 6.3.1 Repealed
  50. 6.3.2Obtain from the electronic integrator the following peak areas: Repealed
  51. EXPRESSION OF RESULTS Repealed
  52. Method of calculation and formula Repealed
  53. 7.1.1The erucic acid content of the sample, expressed in terms of its methyl ester as a percentage of the total fatty acid methyl esters prepared from the sample, is given by: Repealed
  54. 7.1.2If peak areas are obtained in percentages the values for EF and RF may be calculated as follows: Repealed
  55. 7.1.3The method of calculation (7.1.1) assumes that the level of tetracosanoic acid in the sample is negligible. If significant amounts of this acid are shown to be present the value for tetracosanoic acid (L2) obtained from the chromatogram of the fractions containing the remainder of the fatty acid methyl esters must be reduced to: Repealed

1F1

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2F1

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3F1

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4F1

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Signature

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1.1GeneralF1

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1.2Preparation of the sample for analysis in the laboratoryF1

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1.3ContainersF1

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2.1.1F1

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2.1.2F1

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2.2ChemicalsF1

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3.1List of apparatusF1

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3.2Analytical balanceF1

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4.1ResultsF1

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4.2Calculation of the percentageF1

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4.3Number of significant figuresF1

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1SCOPE AND FIELD OF APPLICATIONF1

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2DEFINITIONF1

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3PRINCIPLEF1

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4.1F1

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4.2F1

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4.3F1

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4.4F1

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4.5F1

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4.6F1

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4.7F1

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4.8F1

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4.9F1

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5.1Apparatus for thin-layer chromatography to include, in particular:F1

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5.2F1

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6.1Preparation of fatty-acid methyl estersF1

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6.2.1Preparation of platesF1

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6.2.2Application of methyl estersF1

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6.2.3Development of the platesF1

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6.2.4Separation of the methyl ester fractionsF1

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6.3.1F1

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6.3.2Obtain from the electronic integrator the following peak areas:F1

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7.1.1The erucic acid content of the sample, expressed in terms of its methyl ester as a percentage of the total fatty acid methyl esters prepared from the sample, is given by:F1

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7.1.2If peak areas are obtained in percentages the values for EF and RF may be calculated as follows:F1

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7.1.3The method of calculation (7.1.1) assumes that the level of tetracosanoic acid in the sample is negligible. If significant amounts of this acid are shown to be present the value for tetracosanoic acid (L2) obtained from the chromatogram of the fractions containing the remainder of the fatty acid methyl esters must be reduced to:F1

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