Commission Directive of 25 July 1980 relating to the Community method of analysis for determining the erucic acid content in oils and fats intended to be used as such for human consumption and foodstuffs containing added oils or fats (80/891/EEC) (repealed)
EU Directive 1980/891 · Adopted 25 July 1980 · Extends to United Kingdom
Commission Directive
of 25 July 1980
relating to the Community method of analysis for determining the erucic acid content in oils and fats intended to be used as such for human consumption and foodstuffs containing added oils or fats
(80/891/EEC) (repealed)
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Annotations to the whole text
Textual amendments
Contents
- 1Article 1 Repealed
- 2Article 2 Repealed
- 3Article 3 Repealed
- 4Article 4 Repealed
- Signature
- Annex: THE DETERMINATION OF THE ERUCIC ACID CONTENT IN OILS AND FATS INTENDED TO BE USED AS SUCH FOR HUMAN CONSUMPTION AND IN THE FAT OR OIL COMPONENT OF FOODSTUFFS TO WHICH OILS OR FATS HAVE BEEN ADDED Repealed
- INTRODUCTION Repealed
- SAMPLE PREPARATION Repealed
- 1.1General Repealed
- 1.2Preparation of the sample for analysis in the laboratory Repealed
- 1.3Containers Repealed
- REAGENTS Repealed
- Water Repealed
- 2.1.1Division 2.1.1 Repealed
- 2.1.2Division 2.1.2 Repealed
- 2.2Chemicals Repealed
- APPARATUS Repealed
- 3.1List of apparatus Repealed
- 3.2Analytical balance Repealed
- EXPRESSION OF THE RESULTS Repealed
- 4.1Results Repealed
- 4.2Calculation of the percentage Repealed
- 4.3Number of significant figures Repealed
- DETERMINATION OF ERUCIC ACID Repealed
- 1SCOPE AND FIELD OF APPLICATION Repealed
- 2DEFINITION Repealed
- 3PRINCIPLE Repealed
- REAGENTS Repealed
- 4.1Division 4.1 Repealed
- 4.2Division 4.2 Repealed
- 4.3Division 4.3 Repealed
- 4.4Division 4.4 Repealed
- 4.5Division 4.5 Repealed
- 4.6Division 4.6 Repealed
- 4.7Division 4.7 Repealed
- 4.8Division 4.8 Repealed
- 4.9Division 4.9 Repealed
- APPARATUS Repealed
- 5.1Apparatus for thin-layer chromatography to include, in particular: Repealed
- 5.2Division 5.2 Repealed
- PROCEDURE Repealed
- 6.1Preparation of fatty-acid methyl esters Repealed
- Thin-layer chromatography Repealed
- 6.2.1Preparation of plates Repealed
- 6.2.2Application of methyl esters Repealed
- 6.2.3Development of the plates Repealed
- 6.2.4Separation of the methyl ester fractions Repealed
- Gas-liquid chromatography Repealed
- 6.3.1Division 6.3.1 Repealed
- 6.3.2Obtain from the electronic integrator the following peak areas: Repealed
- EXPRESSION OF RESULTS Repealed
- Method of calculation and formula Repealed
- 7.1.1The erucic acid content of the sample, expressed in terms of its methyl ester as a percentage of the total fatty acid methyl esters prepared from the sample, is given by: Repealed
- 7.1.2If peak areas are obtained in percentages the values for EF and RF may be calculated as follows: Repealed
- 7.1.3The method of calculation (7.1.1) assumes that the level of tetracosanoic acid in the sample is negligible. If significant amounts of this acid are shown to be present the value for tetracosanoic acid (L2) obtained from the chromatogram of the fractions containing the remainder of the fatty acid methyl esters must be reduced to: Repealed
1F1
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2F1
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3F1
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4F1
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Signature
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1.1GeneralF1
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1.2Preparation of the sample for analysis in the laboratoryF1
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1.3ContainersF1
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2.1.1F1
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2.1.2F1
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2.2ChemicalsF1
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3.1List of apparatusF1
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3.2Analytical balanceF1
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4.1ResultsF1
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4.2Calculation of the percentageF1
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4.3Number of significant figuresF1
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1SCOPE AND FIELD OF APPLICATIONF1
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2DEFINITIONF1
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3PRINCIPLEF1
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4.1F1
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4.2F1
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4.3F1
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4.4F1
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4.5F1
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4.6F1
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4.7F1
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4.8F1
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4.9F1
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5.1Apparatus for thin-layer chromatography to include, in particular:F1
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5.2F1
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6.1Preparation of fatty-acid methyl estersF1
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6.2.1Preparation of platesF1
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6.2.2Application of methyl estersF1
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6.2.3Development of the platesF1
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6.2.4Separation of the methyl ester fractionsF1
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6.3.1F1
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6.3.2Obtain from the electronic integrator the following peak areas:F1
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7.1.1The erucic acid content of the sample, expressed in terms of its methyl ester as a percentage of the total fatty acid methyl esters prepared from the sample, is given by:F1
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7.1.2If peak areas are obtained in percentages the values for EF and RF may be calculated as follows:F1
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7.1.3The method of calculation (7.1.1) assumes that the level of tetracosanoic acid in the sample is negligible. If significant amounts of this acid are shown to be present the value for tetracosanoic acid (L2) obtained from the chromatogram of the fractions containing the remainder of the fatty acid methyl esters must be reduced to:F1
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