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Division 8.3 5-MethylfurfuralF1

United Kingdom

Original text. Later amendments are not shown.

Analyte 5-Methylfurfural
Samples Whisky Brandy Rum Cognac 1 Bourbon Cognac 2
No of laboratories participating 11 11 11 11 11 11
No of results accepted (laboratories) 11 11 8 11 10 11
Mean value (mg/l) 0,1 0,2 0,1 0,5 1,7 0,8
Repeatability standard deviation, s r (mg/l) 0,01 0,01 0,02 0,02 0,03 0,07
Repeatability relative standard deviation, RSD r (%) 10,7 6,1 13,6 4,7 2,0 10,0

Repeatability limit, r (mg/l)

(r = 2,8 × s r )

0,0 0,0 0,1 0,1 0,1 0,2
Reproducibility standard deviation, s R (mg/l) 0,03 0,04 0,03 0,18 0,20 0,26
Reproducibility relative standard deviation, RSD R (%) 35 18 22 39 12 35

Reproducibility limit, R (g/l)

(R = 2,8 × s R )

0,1 0,1 0,1 0,5 0,6 0,7

Annotations

Textual amendments

F1

Inserted by Commission Implementing Regulation (EU) 2016/635 of 22 April 2016 amending the Annex to Regulation (EC) No 2870/2000 as regards certain reference methods for the analysis of spirit drinks.