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Division 8.8 Gallic acidF1

United Kingdom

Original text. Later amendments are not shown.

Analyte Gallic acid
Sample Whisky Brandy Rum Cognac 1 Bourbon Cognac 2
No of laboratories participating 16 15 16 16 16 16
No of results accepted (laboratories) 15 14 16 16 16 16
Mean value (mg/l) 1,2 0,4 2,0 6,1 7,3 21,8
Repeatability standard deviation, s r (mg/l) 0,07 0,04 0,06 0,18 0,18 0,60
Repeatability relative standard deviation, RSD r (%) 6,1 8,1 2,9 3,0 2,4 2,8

Repeatability limit, r (mg/l)

(r = 2,8 × s r )

0,2 0,1 0,2 0,5 0,5 1,7
Reproducibility standard deviation, s R (mg/l) 0,43 0,20 0,62 3,3 2,2 7,7
Reproducibility relative standard deviation, RSD R (%) 36 47 31 53 30 35

Reproducibility limit, R (g/l)

(R = 2,8 × s R )

1,2 0,6 1,7 9,1 6,2 21,7

Annotations

Textual amendments

F1

Inserted by Commission Implementing Regulation (EU) 2016/635 of 22 April 2016 amending the Annex to Regulation (EC) No 2870/2000 as regards certain reference methods for the analysis of spirit drinks.