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Seventh Commission Directive of 1 March 1976 establishing Community methods of analysis for the official control of feedingstuffs (76/372/EEC) (repealed)

EU Directive 1976/372 · Adopted 1 March 1976 · Extends to United Kingdom

Original text. legislation.gov.uk does not revise this item, so later amendments are not shown here. Changes made to it are listed under each provision when known.

Seventh Commission Directive

of 1 March 1976

establishing Community methods of analysis for the official control of feedingstuffs

(76/372/EEC) (repealed)

F1. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

Annotations to the whole text

Textual amendments

F1

Repealed by Commission Regulation (EC) No 152/2009 of 27 January 2009 laying down the methods of sampling and analysis for the official control of feed (Text with EEA relevance).

Contents

  1. 1Article 1 Repealed
  2. 2Article 2 Repealed
  3. 3Article 3 Repealed
  4. Annex: DETERMINATION OF AFLATOXIN B1 Repealed
  5. ONE-DIMENSIONAL THIN LAYER CHROMATOGRAPHIC METHOD Repealed
  6. 1Purpose and scope Repealed
  7. 2Principle Repealed
  8. Reagents Repealed
  9. 3.1Division 3.1 Repealed
  10. 3.2Division 3.2 Repealed
  11. 3.3Division 3.3 Repealed
  12. 3.4Division 3.4 Repealed
  13. 3.5Division 3.5 Repealed
  14. 3.6Division 3.6 Repealed
  15. 3.7Division 3.7 Repealed
  16. 3.8Division 3.8 Repealed
  17. 3.9Division 3.9 Repealed
  18. 3.10Division 3.10 Repealed
  19. 3.11Division 3.11 Repealed
  20. 3.12Division 3.12 Repealed
  21. 3.13Division 3.13 Repealed
  22. 3.14Division 3.14 Repealed
  23. 3.15Division 3.15 Repealed
  24. 3.16Division 3.16 Repealed
  25. 3.17Division 3.17 Repealed
  26. 3.18Division 3.18 Repealed
  27. 3.18.1Division 3.18.1 Repealed
  28. 3.18.2Division 3.18.2 Repealed
  29. 3.18.3Division 3.18.3 Repealed
  30. 3.18.4Division 3.18.4 Repealed
  31. 3.18.5Division 3.18.5 Repealed
  32. Apparatus Repealed
  33. 4.1Division 4.1 Repealed
  34. 4.2Division 4.2 Repealed
  35. 4.3Division 4.3 Repealed
  36. 4.4Division 4.4 Repealed
  37. 4.5Division 4.5 Repealed
  38. 4.6Division 4.6 Repealed
  39. 4.7Division 4.7 Repealed
  40. 4.8Division 4.8 Repealed
  41. 4.9Division 4.9 Repealed
  42. 4.10Division 4.10 Repealed
  43. 4.11Division 4.11 Repealed
  44. 4.12Division 4.12 Repealed
  45. Procedure Repealed
  46. 5.1Preparation of the sample (see under‘Observations’, Part C, point 1). Repealed
  47. 5.2Extraction Repealed
  48. 5.3Column clean-up Repealed
  49. 5.4Thin-layer chromatography Repealed
  50. 5.5Quantitative determinations Repealed
  51. 5.5.1Visual measurements Repealed
  52. 5.5.2Measurements by fluorodensitometry Repealed
  53. 5.6Confirmation of the identity of aflatoxin B 1 Repealed
  54. 5.6.1Treatment with sulphuric acid Repealed
  55. Two-dimensional chromatography involving the formation of aflatoxin B1-hemiacetal (aflatoxin B2a) Repealed
  56. 5.6.2.1Division 5.6.2.1 Repealed
  57. 5.6.2.2Division 5.6.2.2 Repealed
  58. 5.6.2.3Division 5.6.2.3 Repealed
  59. Calculation of the results Repealed
  60. 6.1From the visual measurements Repealed
  61. 6.2From the fluorodensitometric measurements Repealed
  62. Preparation and testing of the standard solution (3.16) Repealed
  63. 7.1Determination of the concentration of aflatoxinB1 Repealed
  64. 7.2Testing of chromatographic purity Repealed
  65. 8Repeatability Repealed
  66. 9Reproducibility Repealed
  67. DETERMINATION OF AFLATOXIN B1. HIGH PERFORMANCE LIQUID CHROMATOGRAPHIC METHOD Repealed
  68. 1Purpose and scope Repealed
  69. 2Principle Repealed
  70. Reagents Repealed
  71. 3.1Division 3.1 Repealed
  72. 3.2Division 3.2 Repealed
  73. 3.3Division 3.3 Repealed
  74. 3.4Division 3.4 Repealed
  75. 3.5Division 3.5 Repealed
  76. 3.5.1Division 3.5.1 Repealed
  77. 3.5.2Division 3.5.2 Repealed
  78. 3.5.3Division 3.5.3 Repealed
  79. 3.6Division 3.6 Repealed
  80. 3.7Division 3.7 Repealed
  81. 3.8Division 3.8 Repealed
  82. 3.9Division 3.9 Repealed
  83. 3.10Division 3.10 Repealed
  84. 3.11Division 3.11 Repealed
  85. 3.12Division 3.12 Repealed
  86. 3.12.1Division 3.12.1 Repealed
  87. 3.13Division 3.13 Repealed
  88. 3.13.1Division 3.13.1 Repealed
  89. 3.13.2Division 3.13.2 Repealed
  90. 3.13.3Division 3.13.3 Repealed
  91. 3.13.4Division 3.13.4 Repealed
  92. 3.14Division 3.14 Repealed
  93. 3.14.1Division 3.14.1 Repealed
  94. 3.15Division 3.15 Repealed
  95. 3.15.1Division 3.15.1 Repealed
  96. 3.15.2Division 3.15.2 Repealed
  97. Apparatus Repealed
  98. 4.1Division 4.1 Repealed
  99. 4.2Division 4.2 Repealed
  100. 4.3Division 4.3 Repealed
  101. 4.4Division 4.4 Repealed
  102. 4.5Division 4.5 Repealed
  103. 4.6Division 4.6 Repealed
  104. 4.7Division 4.7 Repealed
  105. 4.8Division 4.8 Repealed
  106. 4.9Division 4.9 Repealed
  107. 4.10Division 4.10 Repealed
  108. 4.11Division 4.11 Repealed
  109. 4.12Division 4.12 Repealed
  110. 4.13Division 4.13 Repealed
  111. 4.14Division 4.14 Repealed
  112. 4.15Division 4.15 Repealed
  113. 4.16Division 4.16 Repealed
  114. 4.17Division 4.17 Repealed
  115. 4.18Division 4.18 Repealed
  116. 4.19Division 4.19 Repealed
  117. 4.20Division 4.20 Repealed
  118. 4.21Division 4.21 Repealed
  119. 4.22Division 4.22 Repealed
  120. 4.23Division 4.23 Repealed
  121. 4.24Division 4.24 Repealed
  122. 4.24.1Division 4.24.1 Repealed
  123. 4.24.2Division 4.24.2 Repealed
  124. Procedure Repealed
  125. 5.1Preparation of the sample. Repealed
  126. 5.2Test portion. Repealed
  127. 5.3Extraction Repealed
  128. Clean-up (the procedure should be carried out without significant interruptions). Repealed
  129. Florisil SEP-PAK purification Repealed
  130. 5.4.1.1Division 5.4.1.1 Repealed
  131. 5.4.1.2Division 5.4.1.2 Repealed
  132. C18 SEP-PAK purification Repealed
  133. 5.4.2.1Division 5.4.2.1 Repealed
  134. 5.4.2.2Division 5.4.2.2 Repealed
  135. 5.5High performance liquid chromatography Repealed
  136. 5.5.1HPLC pump settings Repealed
  137. 5.5.2Post-column pump settings Repealed
  138. 5.5.3Fluorescence detector Repealed
  139. 5.5.4Injector Repealed
  140. 5.5.5Check of chromatographic separation Repealed
  141. 5.5.6Check of the stability of the system Repealed
  142. 5.5.7Check of linearity Repealed
  143. 5.5.8Injection of sample extracts Repealed
  144. Confirmatory test Repealed
  145. 6.1Further treatment of the extract (5.4.2.2) Repealed
  146. 6.2Preparation of derivative and thin layer chromatography: Repealed
  147. 7Calculation of results Repealed
  148. 7.1Division 7.1 Repealed
  149. 8Repeatability: Repealed
  150. 9Reproducibility: Repealed
  151. Observations Repealed
  152. 10.1Precision Repealed
  153. 10.2Stabilization of chloroform (3.1) Repealed
  154. 10.3Accuracy Repealed
  155. OBSERVATIONS CONCERNING METHODS A AND B Repealed
  156. 1Defatting Repealed
  157. 2Reproducibility of the results for Method A Repealed
  158. to AnnexAppendix to Annex Repealed