Division 3.22
United Kingdom
Mobile phase for HPLC: 3,0 g acetic acid (3.18) + 900 ml water (3.1) +50,0 ml solution (3.21) of 1,1,1-trichloro-2-methyl-2-propanol (3.19) in methanol (3.8) (1g/100ml). Adjust pH to 5,0 using ethanolamine (3.20). Make up to 1 000 ml with water (3.1).