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Commission Regulation (EEC) No 000/90 of 17 September 1990 determining Community methods for the analysis of wines (repealed)

EU Regulation No 2676/1990 · Adopted 17 September 1990 · Extends to United Kingdom

Original text. legislation.gov.uk does not revise this item, so later amendments are not shown here. Changes made to it are listed under each provision when known.

Commission Regulation (EEC) No 000/90

of 17 September 1990

determining Community methods for the analysis of wines (repealed)

F1. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

Annotations to the whole text

Textual amendments

F1

Repealed by Commission Regulation (EC) No 606/2009 of 10 July 2009 laying down certain detailed rules for implementing Council Regulation (EC) No 479/2008 as regards the categories of grapevine products, oenological practices and the applicable restrictions.

Contents

  1. 1Article 1 Repealed
  2. 2Article 2 Repealed
  3. 3Article 3 Repealed
  4. 4Article 4 Repealed
  5. 5Article 5 Repealed
  6. 6Article 6 Repealed
  7. Signature
  8. Annex Repealed
  9. DENSITY AND SPECIFIC GRAVITY AT 20 °C Repealed
  10. 1DEFINITIONS Repealed
  11. 2PRINCIPLE OF METHODS Repealed
  12. 3PRELIMINARY TREATMENT OF SAMPLE Repealed
  13. REFERENCE METHOD Repealed
  14. 4.1Apparatus: Repealed
  15. 4.1.1Division 4.1.1 Repealed
  16. 4.1.2Division 4.1.2 Repealed
  17. 4.1.3Division 4.1.3 Repealed
  18. 4.2Calibration of pycnometer Repealed
  19. 4.2.1Method using a twin-pan balance Repealed
  20. Division Repealed
  21. 4.2.2Method using a single-pan balance Repealed
  22. Division Repealed
  23. Method of measurement Repealed
  24. 4.3.1Method using twin-pan balance Repealed
  25. 4.3.2Method using a single-pan balance Repealed
  26. 4.3.3Division 4.3.3 Repealed
  27. 4.3.4Division 4.3.4 Repealed
  28. USUAL METHODS Repealed
  29. Hydrometry Repealed
  30. Apparatus Repealed
  31. 5.1.1.1Division 5.1.1.1 Repealed
  32. 5.1.1.2Division 5.1.1.2 Repealed
  33. 5.1.1.3Division 5.1.1.3 Repealed
  34. Procedure Repealed
  35. 5.1.2.1Method of measurement Repealed
  36. Densimetry using a hydrostatic balance Repealed
  37. Apparatus Repealed
  38. 5.2.1.1Division 5.2.1.1 Repealed
  39. 5.2.1.2Division 5.2.1.2 Repealed
  40. Procedure Repealed
  41. 5.2.2.1Standardization of a hydrostatic balance Repealed
  42. 5.2.2.2Method of measurement Repealed
  43. EXAMPLE OF THE CALCULATION OF THE DENSITY AT 20 °C AND THE 20 °C/20 °C SPECIFIC GRAVITY (REFERENCE METHOD) Repealed
  44. Pycnometry using a twin-pan balance Repealed
  45. Standardization of the pycnometer: Repealed
  46. 1Division 1 Repealed
  47. 2Division 2 Repealed
  48. 3Division 3 Repealed
  49. 4Division 4 Repealed
  50. 6.1.2Determination of the density and specific gravity at 20 °C/20 °C of a dry wine Repealed
  51. Pycnometry using a single-pan balance Repealed
  52. Standardization of the pycnometer: Repealed
  53. 1Division 1 Repealed
  54. 2Division 2 Repealed
  55. 3Division 3 Repealed
  56. 4Division 4 Repealed
  57. 6.2.2Determination of the density and specific gravity at 20° C of a dry wine Repealed
  58. F factors by which the mass of water contained in the Pyrex pycnometer at t °C has to be multiplied in order to calculate the pycnometer volume at 20 °C Repealed
  59. EVALUATION BY REFRACTOMETRY OF THE SUGAR CONCENTRATION IN GRAPE MUSTS, CONCENTRATED GRAPE MUSTS AND RECTIFIED CONCENTRATED GRAPE MUSTS Repealed
  60. 1PRINCIPLE OF THE METHOD Repealed
  61. APPARATUS Repealed
  62. 2.1Abbé refractometer Repealed
  63. PREPARATION OF THE SAMPLE Repealed
  64. 3.1Must and concentrated must Repealed
  65. 3.2Rectified concentrated must Repealed
  66. 4PROCEDURE Repealed
  67. CALCULATION Repealed
  68. Temperature correction Repealed
  69. 5.1.1Division 5.1.1 Repealed
  70. 5.1.2Division 5.1.2 Repealed
  71. 5.2Sugar concentration in must and concentrated must Repealed
  72. 5.3Sugar concentration in rectified concentrated must Repealed
  73. 5.4Refractive index of must, concentrated must and rectified concentrated must Repealed
  74. TABLE ICorrection to be made when the percentage by mass of sucrose has been determined at a temperature different from 20 °C Repealed
  75. ALCOHOLIC STRENGTH BY VOLUME Repealed
  76. 1DEFINITION Repealed
  77. PRINCIPLE OF METHODS Repealed
  78. 2.1Division 2.1 Repealed
  79. 2.2Reference methods: Repealed
  80. Usual methods: Repealed
  81. 2.3.1Division 2.3.1 Repealed
  82. 2.3.2Division 2.3.2 Repealed
  83. 2.3.3Division 2.3.3 Repealed
  84. METHOD OF OBTAINING DISTILLATE Repealed
  85. Apparatus Repealed
  86. 3.1.1Division 3.1.1 Repealed
  87. 3.1.2Division 3.1.2 Repealed
  88. Reagents Repealed
  89. 3.2.1Division 3.2.1 Repealed
  90. 3.3Preparation of sample Repealed
  91. 3.4Procedure Repealed
  92. REFERENCE METHODS Repealed
  93. Measurement of the alcoholic strength of the distillate using a pycnometer Repealed
  94. Apparatus Repealed
  95. 4.1.1Division 4.1.1 Repealed
  96. 4.2Procedure Repealed
  97. Expression of results Repealed
  98. 4.3.1Method of calculation Repealed
  99. 4.3.2Division 4.3.2 Repealed
  100. 4.3.3Division 4.3.3 Repealed
  101. Measurement of the alcoholic strength of wines using a hydrostatic balance Repealed
  102. METHOD OF MEASUREMENT Repealed
  103. 1.1Introduction Repealed
  104. 1.2Object and field of application Repealed
  105. 1.3Principle and definitions Repealed
  106. 1.4Reagents Repealed
  107. 1.4.1Float-cleaning solution (sodium hydroxide, 30 % w/v) Repealed
  108. 1.5Apparatus and equipment Repealed
  109. 1.5.1Division 1.5.1 Repealed
  110. 1.5.2Division 1.5.2 Repealed
  111. 1.5.3Division 1.5.3 Repealed
  112. 1.5.4Division 1.5.4 Repealed
  113. 1.5.5Division 1.5.5 Repealed
  114. 1.6Procedure Repealed
  115. 1.6.1Calibration of the balance Repealed
  116. Calibration of the float Repealed
  117. 1.6.2.1Division 1.6.2.1 Repealed
  118. 1.6.2.2Division 1.6.2.2 Repealed
  119. Control using a water-alcohol solution Repealed
  120. 1.6.3.1Division 1.6.3.1 Repealed
  121. 1.6.3.2Division 1.6.3.2 Repealed
  122. Measurement of the density of a distillate (or of its alcoholic strength if the apparatus allows) Repealed
  123. 1.6.4.1Division 1.6.4.1 Repealed
  124. 1.6.4.2Division 1.6.4.2 Repealed
  125. 1.6.4.3Division 1.6.4.3 Repealed
  126. Cleaning of float and measuring cylinder Repealed
  127. 1.6.5.1Division 1.6.5.1 Repealed
  128. 1.6.5.2Division 1.6.5.2 Repealed
  129. 1.6.5.3Division 1.6.5.3 Repealed
  130. 1.6.5.4Division 1.6.5.4 Repealed
  131. 1.6.6Result Repealed
  132. 2COMPARISON OF MEASUREMENTS MADE USING A HYDROSTATIC BALANCE WITH PROCEDURES OBTAINED USING AN ELECTRONIC DENSIMETER Repealed
  133. 2.1Samples Repealed
  134. 2.2Laboratories Repealed
  135. Equipment Repealed
  136. 2.3.1Division 2.3.1 Repealed
  137. 2.3.2Division 2.3.2 Repealed
  138. 2.4Analysis Repealed
  139. 2.5Result Repealed
  140. Evaluations of the results Repealed
  141. 2.6.1Division 2.6.1 Repealed
  142. 2.6.2Repeatability (r) and reproducibility (R) Repealed
  143. 2.6.3Interlaboratory precision Repealed
  144. 2.6.4Fidelity parameters Repealed
  145. 2.7Conclusion Repealed
  146. Measurement of the alcoholic strength of wines by electronic densimetry using a frequency oscillator Repealed
  147. Method of measurement Repealed
  148. 1.1Title and introduction Repealed
  149. 1.2Purpose and scope Repealed
  150. 1.3Principle and definitions Repealed
  151. Reagents and products Repealed
  152. 1.4.1Reference fluids Repealed
  153. 1.4.2Cleaning and drying products Repealed
  154. Apparatus Repealed
  155. 1.5.1Electronic densimeter using a frequency oscillator Repealed
  156. 1.5.2Controlling the temperature in the measuring cell Repealed
  157. 1.5.3Calibration of the apparatus Repealed
  158. 1.5.4Checking the calibration Repealed
  159. 1.5.5Checks Repealed
  160. 1.6Sampling and preparation of the samples Repealed
  161. 1.7Procedure Repealed
  162. 1.8Expression of results Repealed
  163. 1.9Remarks Repealed
  164. 1.10Precision Repealed
  165. 2Interlaboratory trials. Precision and accuracy on adjuncts Repealed
  166. USUAL METHODS Repealed
  167. Hydrometry Repealed
  168. Apparatus Repealed
  169. 5.1.1.1Division 5.1.1.1 Repealed
  170. 5.1.1.2Division 5.1.1.2 Repealed
  171. 5.1.1.3Division 5.1.1.3 Repealed
  172. 5.1.2Procedure Repealed
  173. Densimetry using a hydrostatic balance Repealed
  174. Apparatus Repealed
  175. 5.2.1.1Division 5.2.1.1 Repealed
  176. 5.2.2Procedure Repealed
  177. 5.2.3Expression of results Repealed
  178. Refractometry Repealed
  179. Apparatus Repealed
  180. 5.3.1.1Division 5.3.1.1 Repealed
  181. 5.3.2Procedure Repealed
  182. 5.3.3Expression of results Repealed
  183. EXAMPLE OF THE CALCULATION OF THE ALCOHOLIC STRENGTH OF A WINE Repealed
  184. Measurement by pycnometer on a twin-pan balance Repealed
  185. 6.1.1Division 6.1.1 Repealed
  186. 6.1.2Weighing of pycnometer filled with distillate Repealed
  187. Calculation of alcoholic strength Repealed
  188. Measurement by pycnometer on a single pan balance Repealed
  189. 6.2.1Division 6.2.1 Repealed
  190. Weighing of the pycnometer filled with distillate Repealed
  191. Calculation of alcoholic strength Repealed
  192. FORMULA FROM WHICH TABLES OF ALCOHOLIC STRENGHTS OF ETHANOL-WATER MIXTURES ARE CALCULATED Repealed
  193. INTERNATIONAL ALCOHOLIC STRENGTH AT 20 °C Repealed
  194. 4TOTAL DRY EXTRACT Repealed
  195. 1DEFINITION Repealed
  196. 2PRINCIPLE OF THE METHOD Repealed
  197. 3METHOD OF CALCULATION Repealed
  198. 4EXPRESSION OF RESULTS Repealed
  199. for the calculation of the content total dry extract (g/l) Repealed
  200. REDUCING SUGARS Repealed
  201. 1DEFINITION Repealed
  202. PRINCIPLE OF THE METHODS Repealed
  203. Clarification Repealed
  204. 2.1.1Division 2.1.1 Repealed
  205. 2.1.2Division 2.1.2 Repealed
  206. 2.1.2.1Division 2.1.2.1 Repealed
  207. 2.1.2.2Division 2.1.2.2 Repealed
  208. 2.2Division 2.2 Repealed
  209. 2.2.1Division 2.2.1 Repealed
  210. 3CLARIFICATION Repealed
  211. Reference method Repealed
  212. Reagents Repealed
  213. 3.1.1.1Division 3.1.1.1 Repealed
  214. 3.1.1.2Division 3.1.1.2 Repealed
  215. 3.1.1.3Division 3.1.1.3 Repealed
  216. 3.1.1.4Division 3.1.1.4 Repealed
  217. 3.1.1.5Division 3.1.1.5 Repealed
  218. Preparation of the anion exchange resin column Repealed
  219. Regeneration of the resin Repealed
  220. 3.1.1.6Division 3.1.1.6 Repealed
  221. 3.1.1.7Division 3.1.1.7 Repealed
  222. Procedure Repealed
  223. 3.1.2.1Dry wines Repealed
  224. 3.1.2.2Musts, mistelles, sweet and semi-sweet wines: Repealed
  225. 1Division 1 Repealed
  226. 2Division 2 Repealed
  227. 3Division 3 Repealed
  228. Usual methods Repealed
  229. Clarification by neutral lead acetate Repealed
  230. 3.2.1.1Reagents Repealed
  231. Procedure Repealed
  232. 3.2.1.2.1Division 3.2.1.2.1 Repealed
  233. 3.2.1.2.2Division 3.2.1.2.2 Repealed
  234. 1Division 1 Repealed
  235. 2Division 2 Repealed
  236. 3Division 3 Repealed
  237. 3.2.2Clarification by zinc 2-hexacyanoferrate Repealed
  238. Reagents Repealed
  239. 3.2.2.1.1Division 3.2.2.1.1 Repealed
  240. 3.2.2.1.2Division 3.2.2.1.2 Repealed
  241. 3.2.2.2Procedure Repealed
  242. 1Division 1 Repealed
  243. 2Division 2 Repealed
  244. 3Division 3 Repealed
  245. 4Division 4 Repealed
  246. DETERMINATION OF SUGARS Repealed
  247. Reagents Repealed
  248. 4.1.1Alkaline copper salt solution: Repealed
  249. 4.1.230 % potassium iodide solution: Repealed
  250. 4.1.325 % sulphuric acid: Repealed
  251. 4.1.45 g/l starch solution: Repealed
  252. 4.2Procedure Repealed
  253. Expression of results Repealed
  254. 4.3.1Calculations Repealed
  255. 4.3.2Repeatability Repealed
  256. 4.3.3Reproducibility Repealed
  257. SUCROSE Repealed
  258. PRINCIPLE OF METHODS Repealed
  259. IDivision I Repealed
  260. IIDivision II Repealed
  261. QUALITATIVE TESTING BY THIN-LAYER CHROMATOGRAPHY Repealed
  262. Equipment Repealed
  263. 2.1.1Division 2.1.1 Repealed
  264. 2.1.2Division 2.1.2 Repealed
  265. 2.1.3Division 2.1.3 Repealed
  266. 2.1.4Division 2.1.4 Repealed
  267. Reagents Repealed
  268. 2.2.1Division 2.2.1 Repealed
  269. 2.2.2Division 2.2.2 Repealed
  270. Developing agent Repealed
  271. Reference solutions Repealed
  272. Procedure Repealed
  273. 2.3.1Preparation of sample Repealed
  274. 2.3.2Obtaining the chromatogram Repealed
  275. 2.4Results Repealed
  276. 3TESTING AND DETERMINATION BY HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY Repealed
  277. Equipment Repealed
  278. 3.1.1Division 3.1.1 Repealed
  279. 1Division 1 Repealed
  280. 2Division 2 Repealed
  281. 3Division 3 Repealed
  282. 4Division 4 Repealed
  283. 5Division 5 Repealed
  284. 6Division 6 Repealed
  285. 7Division 7 Repealed
  286. 3.1.2Division 3.1.2 Repealed
  287. Reagents Repealed
  288. 3.2.1Division 3.2.1 Repealed
  289. 3.2.2Division 3.2.2 Repealed
  290. 3.2.3Division 3.2.3 Repealed
  291. 3.2.4Division 3.2.4 Repealed
  292. Procedure Repealed
  293. 3.3.1Preparation of sample: Repealed
  294. 3.3.2Chromatographic determination Repealed
  295. 3.4Calculations Repealed
  296. 3.4.1Division 3.4.1 Repealed
  297. 3.4.2Division 3.4.2 Repealed
  298. 3.5Expression of results Repealed
  299. GLUCOSE AND FRUCTOSE Repealed
  300. 1DEFINITION Repealed
  301. 2PRINCIPLE OF THE METHOD Repealed
  302. 3APPARATUS Repealed
  303. REAGENTS Repealed
  304. 4.1Division 4.1 Repealed
  305. 4.2Division 4.2 Repealed
  306. 4.3Division 4.3 Repealed
  307. 4.4Division 4.4 Repealed
  308. 4.5Division 4.5 Repealed
  309. PROCEDURE Repealed
  310. 5.1Preparation of sample Repealed
  311. 5.2Determination Repealed
  312. Expression of results Repealed
  313. 5.3.1Calculation Repealed
  314. 5.3.2Repeatability (r) Repealed
  315. 5.3.3Reproducibility (R) Repealed
  316. DETECTING ENRICHMENT OF GRAPE MUSTS, CONCENTRATED GRAPE MUSTS, RECTIFIED CONCENTRATED GRAPE MUSTS AND WINES BY APPLICATION OF NUCLEAR MAGNETIC RESONANCE OF DEUTERIUM (SNIF-NMR/RMN-FINS) Repealed
  317. 1DEFINITION Repealed
  318. 2PRINCIPLE Repealed
  319. PREPARATION OF THE SAMPLE FOR ANALYSIS Repealed
  320. Extraction of ethanol and water in the wine Repealed
  321. 3.1.1Apparatus and reagents Repealed
  322. Procedure Repealed
  323. 3.1.2.1Division 3.1.2.1 Repealed
  324. 3.1.2.2Extraction of the ethanol Repealed
  325. 3.1.2.3Determination of the alcoholic strength of the alcohol extracted Repealed
  326. Fermentation of musts, concentrated musts and rectified concentrated musts Repealed
  327. 3.2.1Apparatus and reagents Repealed
  328. Procedure Repealed
  329. 3.2.2.1Musts Repealed
  330. 3.2.2.2Concentrated musts Repealed
  331. 3.2.2.3Rectified concentrated musts Repealed
  332. Preparation of alcohol sample for NMR measurement Repealed
  333. 3.3.1Reagents Repealed
  334. 3.3.2Procedure Repealed
  335. Preparation of a water sample for the NMR measurement, for the purpose of a possible determination of its isotope ratio Repealed
  336. 3.4.1Reagents Repealed
  337. 3.4.2Procedure Repealed
  338. 4RECORDING OF 2H NMR SPECTRA OF THE ALCOHOL AND THE WATER Repealed
  339. 4.1Apparatus Repealed
  340. Standardization of spectrometer and checks Repealed
  341. 4.2.1Standardization Repealed
  342. 4.2.2Checking the validity of the standardization Repealed
  343. 4.3Conditions for obtaining NMR spectra Repealed
  344. EXPRESSION OF RESULTS Repealed
  345. 5.1Ethanol Repealed
  346. 5.2Water Repealed
  347. 5.3Division 5.3 Repealed
  348. 6INTERPRETATION OF RESULTS Repealed
  349. Addition of beet sugar, cane sugar or maize glucose Repealed
  350. 6.1.1Wines Repealed
  351. 6.1.2Musts, concentrated musts and rectified concentrated masts Repealed
  352. 6.2Addition of a mixture of beet sugar and cane sugar or maize glucose Repealed
  353. ASH CONTENT Repealed
  354. 1DEFINITION Repealed
  355. 2PRINCIPLE OF THE METHOD Repealed
  356. APPARATUS Repealed
  357. 3.1Division 3.1 Repealed
  358. 3.2Division 3.2 Repealed
  359. 3.3Division 3.3 Repealed
  360. 3.4Division 3.4 Repealed
  361. 3.5Division 3.5 Repealed
  362. 3.6Division 3.6 Repealed
  363. 4PROCEDURE Repealed
  364. EXPRESSION OF RESULTS Repealed
  365. 5.1Division 5.1 Repealed
  366. ALKALINITY OF THE ASH Repealed
  367. 1DEFINITION Repealed
  368. 2PRINCIPLE OF THE METHOD Repealed
  369. REAGENTS AND APPARATUS Repealed
  370. 3.1Division 3.1 Repealed
  371. 3.2Division 3.2 Repealed
  372. 3.3Division 3.3 Repealed
  373. 3.4Division 3.4 Repealed
  374. 4PROCEDURE Repealed
  375. 5EXPRESSION OF RESULTS Repealed
  376. CHLORIDES Repealed
  377. 1PRINCIPLE Repealed
  378. APPARATUS Repealed
  379. 2.1Division 2.1 Repealed
  380. 2.2Division 2.2 Repealed
  381. 2.3Division 2.3 Repealed
  382. 2.4Division 2.4 Repealed
  383. 2.5Division 2.5 Repealed
  384. REAGENTS Repealed
  385. 3.1Division 3.1 Repealed
  386. 3.2Division 3.2 Repealed
  387. 3.3Division 3.3 Repealed
  388. PROCEDURE Repealed
  389. 4.1Division 4.1 Repealed
  390. 4.2Division 4.2 Repealed
  391. 4.3Division 4.3 Repealed
  392. EXPRESSION OF RESULTS Repealed
  393. 5.1Calculations Repealed
  394. 5.2Repeatability (r): Repealed
  395. 5.3Reproducibility (R): Repealed
  396. Repealed
  397. SULPHATES Repealed
  398. PRINCIPLE Repealed
  399. 1.1Reference method Repealed
  400. 1.2Quick test method Repealed
  401. REFERENCE METHOD Repealed
  402. Reagents Repealed
  403. 2.1.1Division 2.1.1 Repealed
  404. 2.1.2Division 2.1.2 Repealed
  405. Procedure Repealed
  406. 2.2.1General procedure: Repealed
  407. 2.2.2Division 2.2.2 Repealed
  408. Expression of results Repealed
  409. 2.3.1Calculations: Repealed
  410. 2.3.2Repeatability Repealed
  411. 2.3.3Reproducibility Repealed
  412. QUICK TEST METHOD Repealed
  413. Reagents Repealed
  414. 3.1.1Division 3.1.1 Repealed
  415. 3.1.2Division 3.1.2 Repealed
  416. 3.2Procedure Repealed
  417. TOTAL ACIDITY Repealed
  418. 1DEFINITION Repealed
  419. 2PRINCIPLE OF THE METHOD Repealed
  420. REAGENTS Repealed
  421. 3.1Division 3.1 Repealed
  422. 3.2Division 3.2 Repealed
  423. 3.3Division 3.3 Repealed
  424. APPARATUS Repealed
  425. 4.1Division 4.1 Repealed
  426. 4.2Division 4.2 Repealed
  427. 4.3Division 4.3 Repealed
  428. 4.4Division 4.4 Repealed
  429. PROCEDURE Repealed
  430. Preparation of sample: Repealed
  431. 5.1.1Wines Repealed
  432. 5.1.2Rectified concentrated musts Repealed
  433. Potentiometric titration Repealed
  434. 5.2.1Calibration of pH meter Repealed
  435. 5.2.2Method of measurement Repealed
  436. Titration with indicator (bromothymol blue) Repealed
  437. 5.3.1Preliminary test: end-point colour determination. Repealed
  438. 5.3.2Measurement Repealed
  439. EXPRESSION OF RESULTS Repealed
  440. Method of calculation Repealed
  441. 6.1.1Wines Repealed
  442. 6.1.2Rectified concentrated musts Repealed
  443. 6.2Repeatability (r) for titration with the indicator: Repealed
  444. 6.3Reproducibility (R) for titration with the indicator (5.3): Repealed
  445. VOLATILE ACIDITY Repealed
  446. 1DEFINITION Repealed
  447. 2PRINCIPLE OF THE METHOD Repealed
  448. REAGENTS Repealed
  449. 3.1Division 3.1 Repealed
  450. 3.2Division 3.2 Repealed
  451. 3.3Division 3.3 Repealed
  452. 3.4Division 3.4 Repealed
  453. 3.5Division 3.5 Repealed
  454. 3.6Division 3.6 Repealed
  455. 3.7Division 3.7 Repealed
  456. 3.8Division 3.8 Repealed
  457. APPARATUS Repealed
  458. 4.1Division 4.1 Repealed
  459. 4.2Division 4.2 Repealed
  460. 4.3Division 4.3 Repealed
  461. PROCEDURE Repealed
  462. 5.1Division 5.1 Repealed
  463. 5.2Steam distillation Repealed
  464. 5.3Titration Repealed
  465. EXPRESSION OF RESULTS Repealed
  466. 6.1Method of calculation Repealed
  467. 6.2Repeatability (r) Repealed
  468. 6.3Reproducibility (R) Repealed
  469. 6.4Wine with sorbic acid present Repealed
  470. DETERMINATION OF SALICYLIC ACID ENTRAINED IN THE DISTILLATE FROM THE VOLATILE ACIDITY Repealed
  471. 7.1Principle Repealed
  472. Reagents Repealed
  473. 7.2.1Division 7.2.1 Repealed
  474. 7.2.2Division 7.2.2 Repealed
  475. 7.2.3Division 7.2.3 Repealed
  476. 7.2.4Division 7.2.4 Repealed
  477. Procedure Repealed
  478. 7.3.1Identification of salicylic acid in the volatile acidity distillate. Repealed
  479. 7.3.2Determination of salicylic acid Repealed
  480. 7.3.3Correction to the volatile acidity Repealed
  481. FIXED ACIDITY Repealed
  482. 1PRINCIPLE Repealed
  483. 2EXPRESSION OF RESULTS Repealed
  484. TARTARIC ACID Repealed
  485. PRINCIPLE OF METHODS Repealed
  486. 1.1Reference method Repealed
  487. 1.2Usual method Repealed
  488. REFERENCE METHOD Repealed
  489. Gravimetric method Repealed
  490. Reagents Repealed
  491. 2.1.1.1Division 2.1.1.1 Repealed
  492. 2.1.1.2Division 2.1.1.2 Repealed
  493. 2.1.1.3Division 2.1.1.3 Repealed
  494. Procedure Repealed
  495. 2.1.2.1Wines with no added mesotartaric acid Repealed
  496. 2.1.2.2Wines to which mesotartaric acid has been added Repealed
  497. 2.1.3Expression of results Repealed
  498. Comparative volumetric analysis Repealed
  499. Reagents Repealed
  500. 2.2.1.1Division 2.2.1.1 Repealed
  501. 2.2.1.2Division 2.2.1.2 Repealed
  502. 2.2.1.3Division 2.2.1.3 Repealed
  503. 2.2.1.4Division 2.2.1.4 Repealed
  504. 2.2.2Procedure Repealed
  505. 2.2.3Expression of results Repealed
  506. USUAL METHOD Repealed
  507. Reagents Repealed
  508. For preliminary treatment of the wine Repealed
  509. 3.1.1.1Division 3.1.1.1 Repealed
  510. 3.1.1.2Division 3.1.1.2 Repealed
  511. 3.1.1.3Division 3.1.1.3 Repealed
  512. 3.1.1.4Division 3.1.1.4 Repealed
  513. For the determination of tartaric acid Repealed
  514. 3.1.2.1Division 3.1.2.1 Repealed
  515. 3.1.2.2Division 3.1.2.2 Repealed
  516. 3.1.2.3Division 3.1.2.3 Repealed
  517. 3.1.2.4Division 3.1.2.4 Repealed
  518. 3.1.2.5Division 3.1.2.5 Repealed
  519. 3.1.2.6Division 3.1.2.6 Repealed
  520. 3.1.2.7Division 3.1.2.7 Repealed
  521. 3.1.2.8Division 3.1.2.8 Repealed
  522. 3.1.2.9Division 3.1.2.9 Repealed
  523. 3.1.2.10Division 3.1.2.10 Repealed
  524. Apparatus Repealed
  525. 3.2.1Division 3.2.1 Repealed
  526. 3.2.2Division 3.2.2 Repealed
  527. Procedure Repealed
  528. 3.3.1Preparation of the ion exchange column Repealed
  529. 3.3.2Separation of organic acids Repealed
  530. Determination of tartaric acid Repealed
  531. 3.3.3.1Wines with no added mesotartaric acid Repealed
  532. 3.3.3.2Wines to which mesotartaric acid has been added Repealed
  533. 3.3.4Plotting the calibration curve Repealed
  534. 3.3.5Expression of results Repealed
  535. CITRIC ACID Repealed
  536. 1PRINCIPLE OF THE METHOD Repealed
  537. REAGENTS Repealed
  538. 2.1Division 2.1 Repealed
  539. 2.2Division 2.2 Repealed
  540. 2.3Division 2.3 Repealed
  541. 2.4Division 2.4 Repealed
  542. 2.5Division 2.5 Repealed
  543. APPARATUS Repealed
  544. 3.1Division 3.1 Repealed
  545. 3.2Division 3.2 Repealed
  546. 3.3Division 3.3 Repealed
  547. 4PREPARATION OF THE SAMPLE Repealed
  548. 5PROCEDURE Repealed
  549. 6EXPRESSION OF RESULTS Repealed
  550. 6.1Method of calculation Repealed
  551. 6.2Repeatability (r) Repealed
  552. 6.3Reproducibility (R) Repealed
  553. LACTIC ACID Repealed
  554. 1PRINCIPLE OF THE METHOD Repealed
  555. 1.2Usual method Repealed
  556. REFERENCE METHOD Repealed
  557. Reagents Repealed
  558. 2.1.1Division 2.1.1 Repealed
  559. 2.1.2Division 2.1.2 Repealed
  560. 2.1.3Division 2.1.3 Repealed
  561. 2.1.4Division 2.1.4 Repealed
  562. 2.1.5Division 2.1.5 Repealed
  563. Apparatus Repealed
  564. 2.2.1Division 2.2.1 Repealed
  565. 2.2.2Division 2.2.2 Repealed
  566. 2.2.3Division 2.2.3 Repealed
  567. 2.3Preparation of the sample Repealed
  568. Procedure Repealed
  569. 2.4.1Determination of total lactic acid Repealed
  570. 2.4.2Determination of L-lactic acid and D-lactic acid Repealed
  571. 2.5Expression of results Repealed
  572. 2.5.1Method of calculation Repealed
  573. 2.5.1.1Total lactic acid and D-lactic acid Repealed
  574. 2.5.1.2L-lactic acid Repealed
  575. 2.5.2Repeatability (r) Repealed
  576. 2.5.3Reproducibility (R) Repealed
  577. USUAL METHOD Repealed
  578. 3.1.1For preliminary treatment of the wine Repealed
  579. For the determination of lactic acid Repealed
  580. 3.1.2.1Division 3.1.2.1 Repealed
  581. 3.1.2.2Division 3.1.2.2 Repealed
  582. 3.1.2.3Division 3.1.2.3 Repealed
  583. 3.1.2.4Division 3.1.2.4 Repealed
  584. 3.1.2.5Division 3.1.2.5 Repealed
  585. 3.1.2.6Division 3.1.2.6 Repealed
  586. 3.1.2.7Division 3.1.2.7 Repealed
  587. 3.1.2.8Division 3.1.2.8 Repealed
  588. Apparatus Repealed
  589. 3.2.1Division 3.2.1 Repealed
  590. 3.2.2Division 3.2.2 Repealed
  591. 3.2.3Division 3.2.3 Repealed
  592. Procedure Repealed
  593. 3.3.1Preparation of the ion exchange column Repealed
  594. 3.3.2Separation of organic acids Repealed
  595. 3.3.3Determination of lactic acid Repealed
  596. 3.3.4Plotting the calibration curve Repealed
  597. 3.4Expression of results Repealed
  598. L-MALIC ACID Repealed
  599. 1PRINCIPLE OF THE METHOD Repealed
  600. REAGENTS Repealed
  601. 2.1Division 2.1 Repealed
  602. 2.2Division 2.2 Repealed
  603. 2.3Division 2.3 Repealed
  604. 2.4Division 2.4 Repealed
  605. APPARATUS Repealed
  606. 3.1Division 3.1 Repealed
  607. 3.2Division 3.2 Repealed
  608. 3.3Division 3.3 Repealed
  609. 4PREPARATION OF THE SAMPLE Repealed
  610. 5PROCEDURE Repealed
  611. 6EXPRESSION OF RESULTS Repealed
  612. 6.1Method of calculation Repealed
  613. 6.2Repeatability (r) Repealed
  614. 6.3Reproducibility (R) Repealed
  615. 20D-MALIC ACID Repealed
  616. 1PRINCIPLE Repealed
  617. 2REAGENTS Repealed
  618. Preparation of the solutions Repealed
  619. 1Division 1 Repealed
  620. 2Division 2 Repealed
  621. 3Division 3 Repealed
  622. Stability of the solutions Repealed
  623. APPARATUS Repealed
  624. 3.1Division 3.1 Repealed
  625. 3.2Division 3.2 Repealed
  626. 3.3Division 3.3 Repealed
  627. 4PREPARATION OF THE SAMPLE Repealed
  628. 5PROCEDURE Repealed
  629. 6EXPRESSION OF THE RESULTS Repealed
  630. 7ACCURACY Repealed
  631. 7.1Repeatability Repealed
  632. 7.2Reproducibility Repealed
  633. DOSAGE OF D-MALIC ACID (D(+)-MALIC ACID) IN WINES WITH LOW LEVELS Repealed
  634. 8.1Field of application Repealed
  635. 8.2Principle Repealed
  636. 8.3Reagents Repealed
  637. 8.4Apparatus Repealed
  638. 8.5Preparation of the sample Repealed
  639. 8.6Procedure Repealed
  640. 8.7Internal validation Repealed
  641. Appendix A Repealed
  642. How to deal with side reactions Repealed
  643. Appendix B Repealed
  644. TOTAL MALIC ACID Repealed
  645. 1PRINCIPLE Repealed
  646. APPARATUS Repealed
  647. 2.1Division 2.1 Repealed
  648. 2.2Division 2.2 Repealed
  649. 2.3Division 2.3 Repealed
  650. 2.4Division 2.4 Repealed
  651. REAGENTS Repealed
  652. 3.1Division 3.1 Repealed
  653. 3.2Division 3.2 Repealed
  654. 3.3Division 3.3 Repealed
  655. 3.4Division 3.4 Repealed
  656. 3.5Division 3.5 Repealed
  657. 3.6Division 3.6 Repealed
  658. 3.7Division 3.7 Repealed
  659. 3.8Division 3.8 Repealed
  660. 3.9Division 3.9 Repealed
  661. PROCEDURE Repealed
  662. 4.1Preparation of ion exchange resin Repealed
  663. 4.2Preparation of ion exchange column Repealed
  664. 4.3Separation of DL-malic acid Repealed
  665. 4.4Determination of malic acid Repealed
  666. 4.5Plotting the calibration curve Repealed
  667. 5EXPRESSION OF RESULTS Repealed
  668. Repeatability: Repealed
  669. Reproducibility: Repealed
  670. SORBIC ACID Repealed
  671. PRINCIPLE OF METHODS Repealed
  672. 1.1Determination by ultraviolet absorption spectrophotometry Repealed
  673. 1.2Determination by gas chromatography Repealed
  674. 1.3Identification of traces by thin-layer chromatography Repealed
  675. DETERMINATION BY ULTRAVIOLET ABSORPTION SPECTROPHOTOMETRY Repealed
  676. Reagents Repealed
  677. 2.1.1Division 2.1.1 Repealed
  678. 2.1.2Division 2.1.2 Repealed
  679. 2.1.3Division 2.1.3 Repealed
  680. Apparatus Repealed
  681. 2.2.1Division 2.2.1 Repealed
  682. 2.2.2Division 2.2.2 Repealed
  683. 2.2.3Division 2.2.3 Repealed
  684. Procedure Repealed
  685. 2.3.1Distillation Repealed
  686. 2.3.2Preparation of the calibration curve Repealed
  687. 2.3.3Determination Repealed
  688. Expression of results Repealed
  689. 2.4.1Calculation Repealed
  690. DETERMINATION BY GAS CHROMATOGRAPHY Repealed
  691. Reagents Repealed
  692. 3.1.1Division 3.1.1 Repealed
  693. 3.1.2Division 3.1.2 Repealed
  694. 3.1.3Division 3.1.3 Repealed
  695. Apparatus Repealed
  696. 3.2.1Division 3.2.1 Repealed
  697. 3.2.2Division 3.2.2 Repealed
  698. Procedure Repealed
  699. 3.3.1Preparation of sample to be analysed Repealed
  700. 3.3.2Preparation of the reference solution Repealed
  701. 3.3.3Chromatography Repealed
  702. Expression of results Repealed
  703. 3.4.1Calculation Repealed
  704. IDENTIFICATION OF TRACES OF SORBIC ACID BY THIN LAYER CHROMATOGRAPHY Repealed
  705. Reagents Repealed
  706. 4.1.1Division 4.1.1 Repealed
  707. 4.1.2Division 4.1.2 Repealed
  708. 4.1.3Division 4.1.3 Repealed
  709. 4.1.4Division 4.1.4 Repealed
  710. Apparatus Repealed
  711. 4.2.1Division 4.2.1 Repealed
  712. 4.2.2Division 4.2.2 Repealed
  713. 4.2.3Division 4.2.3 Repealed
  714. 4.2.4Division 4.2.4 Repealed
  715. Procedure Repealed
  716. 4.3.1Preparation of sample to be analysed Repealed
  717. 4.3.2Preparation of dilute reference solutions Repealed
  718. 4.3.3Chromatography Repealed
  719. 4.4Expression of results Repealed
  720. L-ASCORBIC ACID Repealed
  721. 1PRINCIPLE OF METHODS Repealed
  722. 1.1Reference method (fluorimetry) Repealed
  723. 1.2Usual method (colorimetry) Repealed
  724. REFERENCE METHOD (fluorimetric method) Repealed
  725. Reagents Repealed
  726. 2.1.1Division 2.1.1 Repealed
  727. 2.1.2Division 2.1.2 Repealed
  728. 2.1.3Division 2.1.3 Repealed
  729. 2.1.4Division 2.1.4 Repealed
  730. 2.1.5Division 2.1.5 Repealed
  731. 2.1.6Division 2.1.6 Repealed
  732. Apparatus Repealed
  733. 2.2.1Division 2.2.1 Repealed
  734. 2.2.2Division 2.2.2 Repealed
  735. 2.2.3Division 2.2.3 Repealed
  736. 2.2.4Division 2.2.4 Repealed
  737. Procedure Repealed
  738. 2.3.1Preparation of the sample of wine or must Repealed
  739. 2.3.2Preparation of the calibration curve Repealed
  740. 2.3.3Fluorimetric determination Repealed
  741. 2.3.4Expression of results Repealed
  742. USUAL METHOD (colorimetric method) Repealed
  743. Reagents Repealed
  744. 3.1.1Division 3.1.1 Repealed
  745. 3.1.2Division 3.1.2 Repealed
  746. 3.1.3Division 3.1.3 Repealed
  747. 3.1.4Division 3.1.4 Repealed
  748. 3.1.5Division 3.1.5 Repealed
  749. 3.1.6Division 3.1.6 Repealed
  750. 3.1.7Division 3.1.7 Repealed
  751. 3.1.8Division 3.1.8 Repealed
  752. 3.1.9Division 3.1.9 Repealed
  753. 3.1.10Division 3.1.10 Repealed
  754. 3.1.11Division 3.1.11 Repealed
  755. 3.1.12Division 3.1.12 Repealed
  756. 3.1.13Division 3.1.13 Repealed
  757. Apparatus Repealed
  758. 3.2.1Division 3.2.1 Repealed
  759. 3.2.2Division 3.2.2 Repealed
  760. 3.2.3Division 3.2.3 Repealed
  761. 3.2.4Division 3.2.4 Repealed
  762. 3.2.5Division 3.2.5 Repealed
  763. 3.2.6Division 3.2.6 Repealed
  764. 3.2.7Division 3.2.7 Repealed
  765. Procedure Repealed
  766. 3.3.1Oxidation of the L-ascorbic acid to dehydroascorbic acid Repealed
  767. 3.3.2Formation and extraction of the bis(2,4-dinitrophenylhydrazone) derivative of diketogulonic acid Repealed
  768. 3.3.3Separation of the bis(2,4-dinitrophenylhydrazone) by chromatography; this is to be carried out in the 2 hours following the extraction (3.3.2). Repealed
  769. 3.3.4Preparation of the calibration curve Repealed
  770. 3.3.5Expression of results Repealed
  771. 3.3.5.1Calculation Repealed
  772. pH Repealed
  773. 1PRINCIPLE Repealed
  774. APPARATUS Repealed
  775. 2.1Division 2.1 Repealed
  776. Electrodes: Repealed
  777. 2.2.1Division 2.2.1 Repealed
  778. 2.2.2Division 2.2.2 Repealed
  779. 2.2.3Division 2.2.3 Repealed
  780. REAGENTS Repealed
  781. Buffer solutions Repealed
  782. 3.1.1Division 3.1.1 Repealed
  783. 3.1.2Division 3.1.2 Repealed
  784. 3.1.3Division 3.1.3 Repealed
  785. PROCEDURE Repealed
  786. Preparation of the sample for analysis Repealed
  787. 4.1.1Division 4.1.1 Repealed
  788. 4.1.2Division 4.1.2 Repealed
  789. 4.2Zeroing of the apparatus Repealed
  790. 4.3Calibration of the pH meter Repealed
  791. 4.4Determination Repealed
  792. 5EXPRESSION OF RESULTS Repealed
  793. SULPHUR DIOXIDE Repealed
  794. 1DEFINITIONS Repealed
  795. FREE AND TOTAL SULPHUR DIOXIDE Repealed
  796. Principle of the methods Repealed
  797. Reference method Repealed
  798. 2.1.1.1For wines and musts Repealed
  799. 2.1.1.2For rectified concentrated musts Repealed
  800. 2.1.2Rapid method of determination (for wines and musts) Repealed
  801. Reference method Repealed
  802. Apparatus Repealed
  803. 2.2.1.1Division 2.2.1.1 Repealed
  804. 2.2.1.2Division 2.2.1.2 Repealed
  805. Reagents Repealed
  806. 2.2.2.1Division 2.2.2.1 Repealed
  807. 2.2.2.2Division 2.2.2.2 Repealed
  808. 2.2.2.3Division 2.2.2.3 Repealed
  809. 2.2.2.4Division 2.2.2.4 Repealed
  810. Procedure Repealed
  811. 2.2.3.1Determination of free sulphur dioxide Repealed
  812. 2.2.3.2Expression of results Repealed
  813. 2.2.3.2.1Division 2.2.3.2.1 Repealed
  814. Determination of total sulphur dioxide Repealed
  815. 2.2.3.3.1Division 2.2.3.3.1 Repealed
  816. 2.2.3.3.2Division 2.2.3.3.2 Repealed
  817. 2.2.3.4Expression of results Repealed
  818. 2.2.3.4.1Division 2.2.3.4.1 Repealed
  819. 2.2.3.4.2Division 2.2.3.4.2 Repealed
  820. 2.2.3.4.3Division 2.2.3.4.3 Repealed
  821. Rapid method of determination Repealed
  822. Reagents Repealed
  823. 2.3.1.1Division 2.3.1.1 Repealed
  824. 2.3.1.2Division 2.3.1.2 Repealed
  825. 2.3.1.3Division 2.3.1.3 Repealed
  826. 2.3.1.4Division 2.3.1.4 Repealed
  827. 2.3.1.5Division 2.3.1.5 Repealed
  828. Apparatus Repealed
  829. 2.3.2.1Division 2.3.2.1 Repealed
  830. 2.3.2.2Division 2.3.2.2 Repealed
  831. 2.3.2.5Division 2.3.2.5 Repealed
  832. Procedure Repealed
  833. 2.3.3.1Free sulphur dioxide Repealed
  834. 2.3.3.2Sulphur dioxide Repealed
  835. Expression of results Repealed
  836. 2.3.4.1Calculation: Repealed
  837. MOLECULAR SULPHUR DIOXIDE Repealed
  838. 3.1Principle of the method Repealed
  839. 3.2Calculation Repealed
  840. SODIUM Repealed
  841. PRINCIPLE OF THE METHODS Repealed
  842. 1.1Reference method: atomic absorption spectrophotometry Repealed
  843. 1.2Usual method: flame photometry Repealed
  844. REFERENCE METHOD Repealed
  845. Reagents Repealed
  846. 2.1.1Solution containing 1 g of sodium per litre: Repealed
  847. Matrix (model) solution: Repealed
  848. 2.1.3Caesium chloride solution containing 5 % caesium: Repealed
  849. Apparatus Repealed
  850. 2.2.1Division 2.2.1 Repealed
  851. 2.2.2Division 2.2.2 Repealed
  852. Procedure Repealed
  853. 2.3.1Preparation of sample Repealed
  854. 2.3.2Calibration Repealed
  855. 2.3.3Determination Repealed
  856. Expression of results Repealed
  857. 2.4.1Method of calculation Repealed
  858. 2.4.2Repeatability (r) Repealed
  859. 2.4.3Reproducibility (R) Repealed
  860. USUAL METHOD Repealed
  861. Reagents Repealed
  862. 3.1.1Reference solution containing 20 mg sodium per litre Repealed
  863. 3.1.2Dilution solution Repealed
  864. Apparatus Repealed
  865. 3.2.1Division 3.2.1 Repealed
  866. Procedure Repealed
  867. 3.3.1Calibration Repealed
  868. 3.3.2Determination Repealed
  869. Expression of results Repealed
  870. 3.4.1Method of calculation Repealed
  871. 3.4.2Repeatability (r) Repealed
  872. 3.4.3Reproducibility (R) Repealed
  873. POTASSIUM Repealed
  874. PRINCIPLE OF THE METHODS Repealed
  875. 1.1Reference method Repealed
  876. 1.2Usual method Repealed
  877. REFERENCE METHOD Repealed
  878. Reagents Repealed
  879. 2.1.1Solution containing 1 g of potassium per litre: Repealed
  880. Matrix (model) solution: Repealed
  881. 2.1.3Caesium chloride solution containing 5 % caesium: Repealed
  882. Apparatus Repealed
  883. 2.2.1Division 2.2.1 Repealed
  884. 2.2.2Division 2.2.2 Repealed
  885. Procedure Repealed
  886. 2.3.1Preparation of sample Repealed
  887. 2.3.2Calibration Repealed
  888. 2.3.3Determination Repealed
  889. Expression of results Repealed
  890. 2.4.1Method of calculation Repealed
  891. 2.4.2Repeatability (r) Repealed
  892. 2.4.3Reproducibility (R) Repealed
  893. 2.4.4Other ways of expressing results Repealed
  894. USUAL METHOD: FLAME PHOTOMETRY Repealed
  895. Reagents Repealed
  896. 3.1.1Reference solution containing 100 mg potassium per litre Repealed
  897. 3.1.2Dilution solution Repealed
  898. Apparatus Repealed
  899. 3.2.1Division 3.2.1 Repealed
  900. Procedure Repealed
  901. 3.3.1Calibration Repealed
  902. 3.3.2Determination Repealed
  903. Expression of results Repealed
  904. 3.4.1Method of calculation Repealed
  905. 3.4.2Repeatability (r) Repealed
  906. 3.4.3Reproducibility (R) Repealed
  907. 3.4.4Other ways of expressing results: Repealed
  908. MAGNESIUM Repealed
  909. 1PRINCIPLE OF THE METHOD Repealed
  910. REAGENTS Repealed
  911. 2.1Concentrated standard solution containing 1 g magnesium per litre Repealed
  912. Dilute standard solution containing 5 mg magnesium per litre. Repealed
  913. APPARATUS Repealed
  914. 3.1Division 3.1 Repealed
  915. 3.2Division 3.2 Repealed
  916. PROCEDURE Repealed
  917. 4.1Preparation of sample Repealed
  918. 4.2Calibration Repealed
  919. 4.3Determination Repealed
  920. EXPRESSION OF RESULTS Repealed
  921. 5.1Method of calculation Repealed
  922. 5.2Repeatability (r) Repealed
  923. 5.3Reproducibility (R) Repealed
  924. CALCIUM Repealed
  925. 1PRINCIPLE OF THE METHOD Repealed
  926. REAGENTS Repealed
  927. 2.1Standard solution containing 1 g calcium per litre Repealed
  928. Dilute standard solution containing 50 mg calcium per litre Repealed
  929. 2.3Lanthanum chloride solution containing 50 g lanthanum per litre Repealed
  930. APPARATUS Repealed
  931. 3.1Division 3.1 Repealed
  932. 3.2Division 3.2 Repealed
  933. PROCEDURE Repealed
  934. 4.1Preparation of sample Repealed
  935. 4.2Calibration Repealed
  936. 4.3Determination Repealed
  937. EXPRESSION OF RESULTS Repealed
  938. 5.1Method of calculation Repealed
  939. 5.2Repeatability (r) Repealed
  940. 5.3Reproducibility (R) Repealed
  941. IRON Repealed
  942. 1PRINCIPLE OF THE METHODS Repealed
  943. REFERENCE METHOD Repealed
  944. Reagents Repealed
  945. 2.1.1Division 2.1.1 Repealed
  946. 2.1.2Division 2.1.2 Repealed
  947. Apparatus Repealed
  948. 2.2.1Division 2.2.1 Repealed
  949. 2.2.2Division 2.2.2 Repealed
  950. 2.2.3Division 2.2.3 Repealed
  951. Procedure Repealed
  952. 2.3.1Preparation of sample Repealed
  953. 2.3.2Calibration Repealed
  954. 2.3.3Determination Repealed
  955. Expression of results Repealed
  956. 2.4.1Method of calculation Repealed
  957. USUAL METHOD Repealed
  958. Reagents Repealed
  959. 3.1.1Division 3.1.1 Repealed
  960. 3.1.2Division 3.1.2 Repealed
  961. 3.1.3Division 3.1.3 Repealed
  962. 3.1.4Division 3.1.4 Repealed
  963. 3.1.5Division 3.1.5 Repealed
  964. 3.1.6Division 3.1.6 Repealed
  965. 3.1.7Division 3.1.7 Repealed
  966. 3.1.8Division 3.1.8 Repealed
  967. 3.1.9Division 3.1.9 Repealed
  968. 3.1.10Division 3.1.10 Repealed
  969. Apparatus Repealed
  970. 3.2.1Division 3.2.1 Repealed
  971. 3.2.2Division 3.2.2 Repealed
  972. Procedure Repealed
  973. Digestion Repealed
  974. 3.3.1.1For wines with sugar content below 50 g/l: Repealed
  975. For musts and wines with sugar content above 50 g/l: Repealed
  976. 3.3.1.2.1Division 3.3.1.2.1 Repealed
  977. 3.3.1.2.2Division 3.3.1.2.2 Repealed
  978. 3.3.2Blank experiment Repealed
  979. 3.3.3Determination Repealed
  980. 3.3.4Calibration Repealed
  981. Expression of results Repealed
  982. 3.4.1Method of calculation Repealed
  983. COPPER Repealed
  984. 1PRINCIPLE OF THE METHOD Repealed
  985. APPARATUS Repealed
  986. 2.1Division 2.1 Repealed
  987. 2.2Division 2.2 Repealed
  988. 2.3Division 2.3 Repealed
  989. 2.4Division 2.4 Repealed
  990. REAGENTS Repealed
  991. 3.1Division 3.1 Repealed
  992. 3.2Division 3.2 Repealed
  993. 3.3Division 3.3 Repealed
  994. 3.4Division 3.4 Repealed
  995. 3.5Division 3.5 Repealed
  996. PROCEDURE Repealed
  997. 4.1Preparation of sample and determination of copper Repealed
  998. 4.2Calibration Repealed
  999. 4.3Division 4.3 Repealed
  1000. EXPRESSION OF RESULTS Repealed
  1001. 5.1Method of calculation Repealed
  1002. CADMIUM Repealed
  1003. 1Principle Repealed
  1004. 2APPARATUS Repealed
  1005. 2.1Division 2.1 Repealed
  1006. 2.2Division 2.2 Repealed
  1007. 2.3Division 2.3 Repealed
  1008. 3REAGENTS Repealed
  1009. 3.1Division 3.1 Repealed
  1010. 3.2Division 3.2 Repealed
  1011. 3.3Division 3.3 Repealed
  1012. 3.4Division 3.4 Repealed
  1013. 3.5Division 3.5 Repealed
  1014. 3.6Division 3.6 Repealed
  1015. 3.7Division 3.7 Repealed
  1016. PROCEDURE Repealed
  1017. 4.1Preparation of the sample Repealed
  1018. 4.2Preparation of the calibration range of solutions Repealed
  1019. Determination Repealed
  1020. 4.3.1Programming of oven (for guidance only): Repealed
  1021. 4.3.2Atomic absorption measurements: Repealed
  1022. EXPRESSION OF RESULTS Repealed
  1023. 5.1Method of calculation Repealed
  1024. SILVER Repealed
  1025. 1PRINCIPLE OF THE METHOD Repealed
  1026. APPARATUS Repealed
  1027. 2.1Division 2.1 Repealed
  1028. 2.2Division 2.2 Repealed
  1029. 2.3Division 2.3 Repealed
  1030. 2.4Division 2.4 Repealed
  1031. 2.5Division 2.5 Repealed
  1032. 2.6Division 2.6 Repealed
  1033. REAGENTS Repealed
  1034. 3.1Division 3.1 Repealed
  1035. 3.2Division 3.2 Repealed
  1036. 3.3Division 3.3 Repealed
  1037. 3.4Division 3.4 Repealed
  1038. 3.5Division 3.5 Repealed
  1039. PROCEDURE Repealed
  1040. 4.1Preparation of sample Repealed
  1041. 4.2Calibration Repealed
  1042. 4.3Division 4.3 Repealed
  1043. EXPRESSION OF RESULTS Repealed
  1044. 5.1Method of calculation Repealed
  1045. ZINC Repealed
  1046. 1PRINCIPLE OF THE METHOD Repealed
  1047. 2REAGENTS Repealed
  1048. 2.1Division 2.1 Repealed
  1049. 2.2Division 2.2 Repealed
  1050. APPARATUS Repealed
  1051. 3.1Division 3.1 Repealed
  1052. 3.2Division 3.2 Repealed
  1053. 3.3Division 3.3 Repealed
  1054. PROCEDURE Repealed
  1055. 4.1Preparation of sample Repealed
  1056. 4.2Calibration Repealed
  1057. 4.3Determination Repealed
  1058. EXPRESSION OF RESULTS Repealed
  1059. 5.1Method of calculation Repealed
  1060. LEAD Repealed
  1061. 1PRINCIPLE Repealed
  1062. 2APPARATUS Repealed
  1063. 2.1Division 2.1 Repealed
  1064. 2.2Division 2.2 Repealed
  1065. 2.3Division 2.3 Repealed
  1066. 3REAGENTS Repealed
  1067. 3.1Division 3.1 Repealed
  1068. 3.2Division 3.2 Repealed
  1069. 3.3Division 3.3 Repealed
  1070. 3.4Division 3.4 Repealed
  1071. PROCEDURE Repealed
  1072. 4.1Preparation of the sample Repealed
  1073. 4.2Preparation of the calibration range of solutions Repealed
  1074. Determination Repealed
  1075. 4.3.1Programming of oven (for guidance only): Repealed
  1076. 4.3.2Measurements Repealed
  1077. EXPRESSION OF RESULTS Repealed
  1078. 5.1Method of calculation Repealed
  1079. FLUORIDES Repealed
  1080. 1PRINCIPLE Repealed
  1081. APPARATUS Repealed
  1082. 2.1Division 2.1 Repealed
  1083. 2.2Division 2.2 Repealed
  1084. 2.3Division 2.3 Repealed
  1085. 2.4Division 2.4 Repealed
  1086. 2.5Division 2.5 Repealed
  1087. 2.6Division 2.6 Repealed
  1088. REAGENTS Repealed
  1089. 3.1Division 3.1 Repealed
  1090. 3.2Division 3.2 Repealed
  1091. 3.3Division 3.3 Repealed
  1092. PROCEDURE Repealed
  1093. 4.1Direct method Repealed
  1094. 4.2The known additions method Repealed
  1095. 5CALCULATIONS Repealed
  1096. CARBON DIOXIDE Repealed
  1097. PRINCIPLE OF THE METHOD Repealed
  1098. Reference method Repealed
  1099. 1.1.1Still wines (CO2 over pressure ≤ 0,5 × 105 Pa) Repealed
  1100. 1.1.2Sparkling and semi-sparkling wines Repealed
  1101. 1.2Usual method: sparkling and semi-sparkling wines Repealed
  1102. REFERENCE METHOD Repealed
  1103. 2.1Division 2.1 Repealed
  1104. Apparatus Repealed
  1105. 2.1.1.1Division 2.1.1.1 Repealed
  1106. 2.1.1.2Division 2.1.1.2 Repealed
  1107. Reagents Repealed
  1108. 2.1.2.1Division 2.1.2.1 Repealed
  1109. 2.1.2.2Division 2.1.2.2 Repealed
  1110. 2.1.2.3Division 2.1.2.3 Repealed
  1111. 2.1.3Procedure Repealed
  1112. 2.1.4Expression of results Repealed
  1113. Sparkling and semi-sparkling wines Repealed
  1114. Apparatus Repealed
  1115. 2.2.1.1Division 2.2.1.1 Repealed
  1116. 2.2.1.2Division 2.2.1.2 Repealed
  1117. Reagents Repealed
  1118. 2.2.2.1Division 2.2.2.1 Repealed
  1119. 2.2.2.2Division 2.2.2.2 Repealed
  1120. 2.2.2.3Division 2.2.2.3 Repealed
  1121. 2.2.3Procedure Repealed
  1122. 2.2.4Expression of results Repealed
  1123. 2.3Calculation of the theoretical excess pressure Repealed
  1124. USUAL METHOD: SPARKLING AND SEMI-SPARKLING WINES Repealed
  1125. Apparatus Repealed
  1126. 3.1.1Aphrometer Repealed
  1127. 3.2Procedure Repealed
  1128. 3.3Expression of results Repealed
  1129. 4RELATIONSHIP BETWEEN THE PRESSURE AND THE QUANTITY OF CARBON DIOXIDE CONTAINED IN A SEMI-SPARKLING WINE Repealed
  1130. MEASURING EXCESS PRESSURE IN SPARKLING AND SEMI-SPARKLING WINES Repealed
  1131. 1PRINCIPLE Repealed
  1132. 2EQUIPMENT Repealed
  1133. 2.1Bottles with capsules Repealed
  1134. 2.2Bottles with corks Repealed
  1135. 3PROCEDURE Repealed
  1136. 3.1Bottles with capsules Repealed
  1137. 3.2Bottles with corks Repealed
  1138. 4EXPRESSION OF RESULTS Repealed
  1139. 5CONTROLLING THE RESULTS Repealed
  1140. CYANIDE DERIVATIVES Repealed
  1141. 1PRINCIPLE Repealed
  1142. APPARATUS Repealed
  1143. 2.1Distillation apparatus Repealed
  1144. 2.2Division 2.2 Repealed
  1145. 2.3Division 2.3 Repealed
  1146. 2.4Division 2.4 Repealed
  1147. 2.5Division 2.5 Repealed
  1148. REAGENTS Repealed
  1149. 3.1Division 3.1 Repealed
  1150. 3.2Division 3.2 Repealed
  1151. 3.3Division 3.3 Repealed
  1152. 3.4Division 3.4 Repealed
  1153. 3.5Division 3.5 Repealed
  1154. 3.6Division 3.6 Repealed
  1155. PROCEDURE Repealed
  1156. 4.1Distillation Repealed
  1157. 4.2Measurement Repealed
  1158. DETERMINING THE CALIBRATION CURVE Repealed
  1159. 5.1Argentometric titration of the potassium cyanide Repealed
  1160. Standard curve Repealed
  1161. 5.2.1Preparation of standard solutions Repealed
  1162. 5.2.2Titration Repealed
  1163. 6EXPRESSION OF RESULTS Repealed
  1164. 6.1Method of calculation Repealed
  1165. ALLYL ISOTHIOCYANATE Repealed
  1166. 1PRINCIPLE OF THE METHOD Repealed
  1167. REAGENTS Repealed
  1168. 2.1Division 2.1 Repealed
  1169. 2.2Division 2.2 Repealed
  1170. 2.3Division 2.3 Repealed
  1171. APPARATUS Repealed
  1172. 3.1Division 3.1 Repealed
  1173. 3.2Division 3.2 Repealed
  1174. 3.3Division 3.3 Repealed
  1175. 3.4Division 3.4 Repealed
  1176. 3.5Division 3.5 Repealed
  1177. 3.6Division 3.6 Repealed
  1178. 4PROCEDURE Repealed
  1179. CHROMATIC PROPERTIES Repealed
  1180. 1WINES AND MUSTS Repealed
  1181. 1.1Definitions Repealed
  1182. Principle of the methods Repealed
  1183. 1.2.1Reference method Repealed
  1184. 1.2.2Usual method (applicable to red and rosé wines) Repealed
  1185. Reference method Repealed
  1186. Apparatus Repealed
  1187. 1.3.1.1Division 1.3.1.1 Repealed
  1188. 1.3.1.2Division 1.3.1.2 Repealed
  1189. Procedure Repealed
  1190. 1.3.2.1Preparation of the sample Repealed
  1191. 1.3.2.2Measurements Repealed
  1192. 1.3.3Calculations Repealed
  1193. Expression of results Repealed
  1194. 1.3.4.1Division 1.3.4.1 Repealed
  1195. 1.3.4.2Division 1.3.4.2 Repealed
  1196. 1.3.4.3Division 1.3.4.3 Repealed
  1197. Usual method Repealed
  1198. Apparatus Repealed
  1199. 1.4.1.1Division 1.4.1.1 Repealed
  1200. 1.4.1.2Division 1.4.1.2 Repealed
  1201. 1.4.2Preliminary preparation of the sample Repealed
  1202. 1.4.3Procedure Repealed
  1203. Expression of results Repealed
  1204. 1.4.4.1Calculations Repealed
  1205. Transformation of absorbences to transmittances (T%) Repealed
  1206. Method of use Repealed
  1207. Example: Repealed
  1208. RECTIFIED CONCENTRATED MUSTS Repealed
  1209. 2.1Principle of the method Repealed
  1210. Apparatus Repealed
  1211. 2.2.1Division 2.2.1 Repealed
  1212. 2.2.2Division 2.2.2 Repealed
  1213. 2.2.3Division 2.2.3 Repealed
  1214. Procedure Repealed
  1215. 2.3.1Preparation of the sample Repealed
  1216. 2.3.2Determination of absorbence Repealed
  1217. 2.4Expression of results Repealed
  1218. FOLIN-CIOCALTEU INDEX Repealed
  1219. 1DEFINITION Repealed
  1220. 2PRINCIPLE OF THE METHOD Repealed
  1221. 3REAGENTS Repealed
  1222. 3.1Folin-Ciocalteu reagent Repealed
  1223. 3.2Division 3.2 Repealed
  1224. 4APPARATUS Repealed
  1225. 4.1Division 4.1 Repealed
  1226. 4.2Division 4.2 Repealed
  1227. PROCEDURE Repealed
  1228. 5.1Red wine Repealed
  1229. 5.2White wine Repealed
  1230. Rectified concentrated must Repealed
  1231. 5.3.1Preparation of sample Repealed
  1232. 5.3.2Measurement Repealed
  1233. EXPRESSION OF RESULTS Repealed
  1234. 6.1Method of calculation Repealed
  1235. 6.2Repeatability Repealed
  1236. SPECIAL METHODS OF ANALYSIS FOR RECTIFIED CONCENTRATED GRAPE MUST Repealed
  1237. TOTAL CATIONS Repealed
  1238. 1PRINCIPLE OF THE METHOD Repealed
  1239. APPARATUS Repealed
  1240. 2.1Division 2.1 Repealed
  1241. 2.2Division 2.2 Repealed
  1242. 2.3Division 2.3 Repealed
  1243. REAGENTS Repealed
  1244. 3.1Division 3.1 Repealed
  1245. 3.2Division 3.2 Repealed
  1246. 3.3Division 3.3 Repealed
  1247. PROCEDURE Repealed
  1248. 4.1Preparation of sample Repealed
  1249. 4.2Preparation of the ion exchange column Repealed
  1250. 4.3Ion exchange Repealed
  1251. 5EXPRESSION OF RESULTS Repealed
  1252. 5.1Division 5.1 Repealed
  1253. CONDUCTIVITY Repealed
  1254. 1PRINCIPLE OF THE METHOD Repealed
  1255. APPARATUS Repealed
  1256. 2.1Division 2.1 Repealed
  1257. 2.2Division 2.2 Repealed
  1258. REAGENTS Repealed
  1259. 3.1Division 3.1 Repealed
  1260. 3.2Division 3.2 Repealed
  1261. PROCEDURE Repealed
  1262. 4.1Preparation of the sample to be analysed Repealed
  1263. 4.2Determination of conductivity Repealed
  1264. 5EXPRESSION OF RESULTS Repealed
  1265. 5.1Calculations Repealed
  1266. HYDROXYMETHYLFURFURAL (HMF) Repealed
  1267. PRINCIPLE OF THE METHODS Repealed
  1268. 1.1Colorimetric method Repealed
  1269. 1.2High-performance liquid chromatography (HPLC) Repealed
  1270. COLORIMETRIC METHOD Repealed
  1271. Apparatus Repealed
  1272. 2.1.1Division 2.1.1 Repealed
  1273. 2.1.2Division 2.1.2 Repealed
  1274. Reagents Repealed
  1275. 2.2.1Barbituric acid, 0,5 % solution (m/v). Repealed
  1276. 2.2.2Paratoluidine solution, 10 % (m/v). Repealed
  1277. 2.2.3Ethanal (acetaldehyde), CH3CHO, 1 % (m/v) aqueous solution. Repealed
  1278. 2.2.4Hydroxymethylfurfural, C6O3H6, 1 g/l aqueous solution. Repealed
  1279. Procedure Repealed
  1280. 2.3.1Preparation of sample Repealed
  1281. 2.3.2Colorimetric determination Repealed
  1282. 2.3.3Preparation of the calibration curve Repealed
  1283. 2.4Expression of results Repealed
  1284. 2.4.1Method of calculation Repealed
  1285. HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY Repealed
  1286. Apparatus Repealed
  1287. 3.1.1High-performance liquid chromatograph equipped with: Repealed
  1288. 3.1.2Division 3.1.2 Repealed
  1289. Reagents Repealed
  1290. 3.2.1Division 3.2.1 Repealed
  1291. 3.2.2Division 3.2.2 Repealed
  1292. 3.2.3Division 3.2.3 Repealed
  1293. 3.2.4Division 3.2.4 Repealed
  1294. 3.2.5Division 3.2.5 Repealed
  1295. Procedure Repealed
  1296. 3.3.1Preparation of sample Repealed
  1297. 3.3.2Chromatographic determination Repealed
  1298. 3.4EXPRESSION OF RESULTS Repealed
  1299. 3.4.1Method of calculation Repealed
  1300. HEAVY METALS Repealed
  1301. PRINCIPLE OF THE METHODS Repealed
  1302. IRapid method for evaluation of heavy metals Repealed
  1303. IIDetermination of lead content by atomic absorption spectrophotometry Repealed
  1304. RAPID METHOD FOR EVALUATION OF HEAVY METALS Repealed
  1305. Reagents Repealed
  1306. 2.1.1Dilute hydrochloric acid, 70 % (m/v). Repealed
  1307. 2.1.2Dilute hydrochloric acid, 20 % (m/v). Repealed
  1308. 2.1.3Division 2.1.3 Repealed
  1309. 2.1.4pH 3,5 buffer solution. Repealed
  1310. 2.1.5Division 2.1.5 Repealed
  1311. 2.1.6Division 2.1.6 Repealed
  1312. 2.1.7Thioacetamide reagent. Repealed
  1313. 2.1.8Solution containing 0,002 g/l of lead. Repealed
  1314. 2.2Procedure Repealed
  1315. 2.3Calculations Repealed
  1316. DETERMINATION OF LEAD CONTENT BY ATOMIC ABSORPTION SPECTROPHOTOMETRY Repealed
  1317. Apparatus Repealed
  1318. 3.1.1Division 3.1.1 Repealed
  1319. 3.1.2Division 3.1.2 Repealed
  1320. Reagents Repealed
  1321. 3.2.1Dilute acetic acid. Repealed
  1322. 3.2.2Division 3.2.2 Repealed
  1323. 3.2.3Division 3.2.3 Repealed
  1324. 3.2.4Division 3.2.4 Repealed
  1325. Procedure Repealed
  1326. 3.3.1Preparation of solution to be examined Repealed
  1327. 3.3.2Preparation of reference solutions Repealed
  1328. 3.3.3Control Repealed
  1329. 3.3.4Determination Repealed
  1330. 3.4Expression of results Repealed
  1331. 3.4.1Calculations Repealed
  1332. (e)CHEMICAL DETERMINATION OF ETHANOL Repealed
  1333. 1PRINCIPLE OF THE METHOD Repealed
  1334. APPARATUS Repealed
  1335. 2.1Division 2.1 Repealed
  1336. REAGENTS Repealed
  1337. 3.1Potassium dichromate solution. Repealed
  1338. 3.2Iron (II) ammonium sulphate solution. Repealed
  1339. 3.3Potassium permanganate solution. Repealed
  1340. 3.4Dilute sulphuric acid, 1:2 (v/v). Repealed
  1341. 3.5Ferrous orthophenanthroline reagent. Repealed
  1342. PROCEDURE Repealed
  1343. 4.1Distillation Repealed
  1344. 4.2Oxidation Repealed
  1345. 4.3Titration Repealed
  1346. 5EXPRESSION OF RESULTS Repealed
  1347. 5.1Method of calculation Repealed
  1348. MESO-INOSITOL, SCYLLO-INOSITOL AND SUCROSE Repealed
  1349. 1PRINCIPLE Repealed
  1350. REAGENTS Repealed
  1351. 2.1Division 2.1 Repealed
  1352. 2.2Division 2.2 Repealed
  1353. 2.3Division 2.3 Repealed
  1354. 2.4Division 2.4 Repealed
  1355. 2.5Division 2.5 Repealed
  1356. APPARATUS Repealed
  1357. 3.1Division 3.1 Repealed
  1358. 3.2Division 3.2 Repealed
  1359. 3.3Division 3.3 Repealed
  1360. 3.4Division 3.4 Repealed
  1361. 3.5Division 3.5 Repealed
  1362. 3.6Division 3.6 Repealed
  1363. 3.7Division 3.7 Repealed
  1364. 4METHOD OF OPERATION Repealed
  1365. CALCULATION OF RESULTS Repealed
  1366. 5.1Division 5.1 Repealed
  1367. EXPRESSION OF RESULTS Repealed
  1368. 6.1Division 6.1 Repealed
  1369. DETERMINATION OF THE ISOTOPIC RATIO 18O/16O OF THE WATER CONTENT IN WINES Repealed
  1370. DESCRIPTION OF THE METHOD Repealed
  1371. 1Method objective Repealed
  1372. 2Principle Repealed
  1373. 3Reagents Repealed
  1374. 4Laboratory equipment Repealed
  1375. Experimental determinations Repealed
  1376. Manual method Repealed
  1377. Operational mode of the equilibration method Repealed
  1378. Degasing of the ramp Repealed
  1379. Equilibration of the water and the CO2 Repealed
  1380. Transfer of the CO2 exchanged in the measuring cells Repealed
  1381. 5.2Use of an automatic exchange apparatus Repealed
  1382. 6Calculation and expression of the results Repealed
  1383. 7Fidelity Repealed
  1384. 44DETERMINATION OF ETHYL CARBAMATE IN WINE: SELECTIVE DETECTION METHOD USING GAS CHROMATOGRAPHY/MASS SPECTROMETRY Repealed
  1385. APrinciple Repealed
  1386. BApparatus and chromatographic conditions (example) Repealed
  1387. CReagents Repealed
  1388. DPreparation of the test sample Repealed
  1389. EExtraction Repealed
  1390. FGC/MS analysis Repealed
  1391. GCollaborative analysis Repealed
  1392. DETERMINATION BY ISOTOPE MASS SPECTROMETRY OF THE 13C/12C RATIO IN WINE ETHANOL OR ETHANOL OBTAINED BY THE FERMENTATION OF MUSTS, CONCENTRATED MUSTS OR RECTIFIED CONCENTRATED MUSTS Repealed
  1393. 1FIELD OF APPLICATION Repealed
  1394. 2REFERENCE STANDARDS Repealed
  1395. 3TERMS AND DEFINITIONS Repealed
  1396. 4PRINCIPLE Repealed
  1397. 5REAGENTS Repealed
  1398. APPARATUS AND EQUIPMENT Repealed
  1399. 6.1Isotope ratio mass spectrometer (IRMS) Repealed
  1400. 6.2Combustion apparatus Repealed
  1401. 6.2.1Continuous-flow systems Repealed
  1402. 6.2.2Separate preparation system Repealed
  1403. 7PREPARATION OF SAMPLES FOR TESTS Repealed
  1404. 8PROCEDURE Repealed
  1405. 9CALCULATION Repealed
  1406. 10QUALITY ASSURANCE AND CONTROL Repealed
  1407. 11PERFORMANCE CHARACTERISTICS OF THE METHOD (Accuracy) Repealed
  1408. 11.1Joint study on distillates Repealed
  1409. 11.2Interlaboratory study on two wines and one alcohol Repealed
  1410. 11.3Results of the exercises carried out to monitor proficiency in performing isotopic tests Repealed
  1411. 11.4Limits of repeatability and reproducibility Repealed